2,2-二氯-1-[4-(1,1-二甲基乙基)苯基]乙烷-1-酮合成路线 （共 6 条）
反应条件
PhMgI in tetrahydrofuran
T=20°C; 1 h; Inert atmosphere;
参考文献
Essa, Ali H.; Lerrick, Reinner I.; Tuna, Floriana; Harrington, Ross W.; Clegg, William; Hall, Michael J.
Chemical Communications, 2013 , vol. 49, # 27 p. 2756 - 2758
反应条件
hydrogenchloride; carbon disulfide; aluminium trichloride
参考文献
Mobil Oil Corporation
Patent: US3939218 A1, 1976 ;
反应条件
hydrogenchloride; carbon disulfide; aluminium trichloride
参考文献
Mobil Oil Corporation
Patent: US3968168 A1, 1976 ;
反应条件
in tetrahydrofuran
T=20°C; 1 h; Inert atmosphere;
参考文献
Essa, Ali H.; Lerrick, Reinner I.; Tuna, Floriana; Harrington, Ross W.; Clegg, William; Hall, Michael J.
Chemical Communications, 2013 , vol. 49, # 27 p. 2756 - 2758
反应条件
in tetrahydrofuran
T=20°C; 1 h; Inert atmosphere;
参考文献
Essa, Ali H.; Lerrick, Reinner I.; Tuna, Floriana; Harrington, Ross W.; Clegg, William; Hall, Michael J.
Chemical Communications, 2013 , vol. 49, # 27 p. 2756 - 2758
反应条件
1: AlCl3, aluminium chloride / dichloromethane / 96 h / -30 °C / |Inert atmosphere
2: PhMgI / tetrahydrofuran / 1 h / 20 °C / |Inert atmosphere
View Scheme
参考文献
Essa, Ali H.; Lerrick, Reinner I.; Tuna, Floriana; Harrington, Ross W.; Clegg, William; Hall, Michael J.
Chemical Communications, 2013 , vol. 49, # 27 p. 2756 - 2758
