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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
8-溴-1-辛醇
合成路线
（共 110 条）
50816-19-8
8-溴-1-辛醇
→
反应条件
55110-79-7
反应条件
1.1: 5 h / 10 - 20 °C 2.1: 93 percent / ethylenediamine / dimethylsulfoxide / 3 h / 15 - 20 °C 3.1: benzene / 6 h / 20 °C 3.2: 71 percent / I2 / benzene; hexane / 20 °C 4.1: 73 percent / Pd(PPh3)4 / benzene / 10 - 20 °C 5.1: 82 percent / PPTs / methanol / 24 h / 20 °C View Scheme
参考文献
Cardillo, Giuliana; Orena, Mario; Porzi, Gianni; Sandri, Sergio
Gazzetta Chimica Italiana, 1980 , vol. 110, # 9/10 p. 523 - 526
50816-19-8
8-溴-1-辛醇
→
反应条件
56606-79-2
反应条件
1: PCC, celite / CH2Cl2 / 3 h / Ambient temperature 2: tetrahydrofuran / 0.5 h / -78 °C 3: Jones reagent / acetone / 0.08 h 4: sodium iodide / butan-2-one / 3 h / Heating 5: tributyltin hydride, AIBN / benzene / 3 h / Heating View Scheme
参考文献
Porter,N.A.; Chang,V.H.; Magnin,D.R.
Journal of the American Chemical Society, 1988 , vol. 110, p. 3554
50816-19-8
8-溴-1-辛醇
→
反应条件
57491-34-6
(3E,13E)-1-乙酰氧基-3,13-十八碳二烯
反应条件
1.1: 3 h 2.1: n-butyllithium / tetrahydrofuran 2.2: tetrahydrofuran; hexamethylphosphoric acid triamide / 1 h / 20 °C 3.1: lithium; ethylamine / 1 h / -5 °C 4.1: p-toluenesulfonic acid / ethanol / 3 h / Heating 5.1: iodine; triphenylphosphine; imidazole / diethyl ether; acetonitrile / 1 h / 0 °C 6.1: n-butyllithium / tetrahydrofuran 6.2: tetrahydrofuran; hexamethylphosphoric acid triamide / 1 h / 20 °C 7.1: lithium; ethylamine / 1 h / -5 °C 8.1: p-toluenesulfonic acid / ethanol / 3 h / Heating 9.1: 93 percent / pyridine / 0.5 h / 20 °C View Scheme
参考文献
Armstrong-Chong, Rosemary J.; Matthews, Kristopher; Chong, J. Michael
Tetrahedron, 2004 , vol. 60, # 45 p. 10239 - 10244
50816-19-8
8-溴-1-辛醇
+
144-55-8
碳酸氢钠
→
反应条件
593-12-4
1-溴-8-氟辛烷
反应条件
Diethylaminosulfur trifluoride in hexane; dichloromethane; ethyl acetate
参考文献
Research Foundation of State University of New York
Patent: US4455441 A1, 1984 ;
50816-19-8
8-溴-1-辛醇
→
反应条件
593-12-4
1-溴-8-氟辛烷
反应条件
diethylamino-sulfur trifluoride T=20 - 50°C; Inert atmosphere;
参考文献
Tremblay, Amy E.; Tan, Nigel; Whittle, Ed; Hodgson, Derek J.; Dawson, Brian; Buist, Peter H.; Shanklin, John
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 6 p. 1322 - 1328
50816-19-8
8-溴-1-辛醇
→
反应条件
60037-69-6
9-十四碳炔-1-醇
反应条件
1: p-TsOH / diethyl ether 2: 1.) 2M BuLi / 1.) hexane, HMPT, 0 deg C, 30 min, 2.)THF, r. t., 12 h 3: p-TsOH / methanol / 2 h / Heating View Scheme
参考文献
Rossi, Renzo; Carpita, Adriano; Gaudenzi, Loretta; Quirici, Maria Grazia
Gazzetta Chimica Italiana, 1980 , vol. 110, # 4 p. 237 - 246
50816-19-8
8-溴-1-辛醇
+
17689-03-1
→
反应条件
60037-69-6
9-十四碳炔-1-醇
反应条件
暂无反应条件数据
参考文献
Verba, G. G.; Bikulova, L. M.; Abduvakhabod, A. A.
Chemistry of Natural Compounds, 1988 , vol. 24, # 1 p. 130 - 131
Khimiya Prirodnykh Soedinenii, 1988 , vol. 24, # 1 p. 143 - 145
50816-19-8
8-溴-1-辛醇
→
反应条件
6008-27-1
反应条件
2: 1) LDA, 2) HMPA / 1) THF, -78 deg C 3: 83 percent / TBAF / tetrahydrofuran 4: 100 percent / O2, sensitox / CH2Cl2 5: 45 percent / collidinium p-toluene sulfonate / benzene / Heating View Scheme
参考文献
Wasserman; DeSimone; Ho; McCarthy; Spencer Prowse; Spada
Tetrahedron Letters, 1992 , vol. 33, # 47 p. 7207 - 7210
50816-19-8
8-溴-1-辛醇
→
反应条件
61618-01-7
反应条件
1: 93 percent / Amberlyst H-15 / CH2Cl2 / 1 h / 0 °C 2: 91 percent / NaI / acetone 3: 1.) (i-C3H7)2NLi / 1.) THF, n-hexane, room temp., 3 h, 2.) 55 deg C, 12 h 4: 92 percent / Amberlyst H-15 / methanol / 1 h / 45 °C 5: 95 percent / LiAlH4 / tetrahydrofuran / 1 h / Heating 6: MnO2 / CH2Cl2 / 6 h / Ambient temperature View Scheme
参考文献
Cardillo, Giuliana; Orena, Mario; Porzi, Gianni; Sandri, Sergio
Gazzetta Chimica Italiana, 1980 , vol. 110, # 9/10 p. 523 - 526
50816-19-8
8-溴-1-辛醇
→
反应条件
51323-71-8
反应条件
1: 91 percent / PPTS / CH2Cl2 / 2 h / Ambient temperature 2: 1.) Li2CuCl4, 2.) PTSA / 1.) THF, room temperature, 12 h, 2.) CH3OH, room temperature, 6 h 3: pyridine / CH2Cl2 / 12 h / Ambient temperature View Scheme
参考文献
Nakashima, Hideki; Hirata, Norihiko; Iwamura, Takeru; Yamagiwa, Yoshiro; Kamikawa, Tadao
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 19 p. 2849 - 2858
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