4-苄氧基苯甲醛-alpha-D1合成路线 （共 6 条）
反应条件
hydrogenchloride in ethanol
T=70°C; 2 h;
参考文献
Al-Ani, Hakim A. M.; Dewick, Paul M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , p. 2831 - 2838
反应条件
1: 1.) 60percent perchloric acid / 1.) 60 deg C, 1 h, 2.) water, 90 deg C, 1 h
2: 40 percent / sodium hydride, D2O / dimethylformamide / 1.) 40 deg C, 1 h, 2.) 5 min
3: 95 percent / 2M HCl / ethanol / 2 h / 70 °C
View Scheme
参考文献
Al-Ani, Hakim A. M.; Dewick, Paul M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , p. 2831 - 2838
反应条件
1: 40 percent / sodium hydride, D2O / dimethylformamide / 1.) 40 deg C, 1 h, 2.) 5 min
2: 95 percent / 2M HCl / ethanol / 2 h / 70 °C
View Scheme
参考文献
Al-Ani, Hakim A. M.; Dewick, Paul M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , p. 2831 - 2838
反应条件
1: LiAl(2)H4 / tetrahydrofuran / 20 °C
2: MnO2 / benzene / 50 °C
View Scheme
参考文献
Suzuki; Umezawa; Shimada
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 24 p. 3252 - 3257
反应条件
1: K2CO3
2: LiAl(2)H4 / tetrahydrofuran / 20 °C
3: MnO2 / benzene / 50 °C
View Scheme
参考文献
Suzuki; Umezawa; Shimada
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 24 p. 3252 - 3257
反应条件
1: K2CO3
2: LiAl(2)H4 / tetrahydrofuran / 20 °C
3: MnO2 / benzene / 50 °C
View Scheme
参考文献
Suzuki; Umezawa; Shimada
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 24 p. 3252 - 3257
