2-溴-1-(3,5-二甲氧基苯基)乙酮合成路线 (共 5 条)
反应条件
copper(ll) bromide in chloroform; ethyl acetate
16 h; Reflux;
参考文献
Kim, Ikyon; Choi, Jihyun
Organic and Biomolecular Chemistry, 2009 , vol. 7, # 13 p. 2788 - 2795
参考文献
Chen, Li; Ding, Qingjie; Gillespie, Paul; Kim, Kyungjin; Lovey, Allen John; McComas, Warren William; Mullin JR., John Guilfoye; Perrotta, Agostino
Patent: US2002/151554 A1, 2002 ;
反应条件
1: diethyl ether / und Erwaermen des Reaktionsprodukts mit Essigsaeure und wss.H2SO4
2: CS2; bromine
View Scheme
参考文献
Abe et al.
Yakugaku Zasshi, 1956 , vol. 76, p. 1094
Chem.Abstr., 1957 , p. 2636
反应条件
water; hydrogen bromide
参考文献
Abe et al.
Yakugaku Zasshi, 1956 , vol. 76, p. 1094
Chem.Abstr., 1957 , p. 2636
反应条件
1: aluminum oxide / anhydrous xylene / 16 h / Reflux
2: boron tribromide / dichloromethane / 0 - 20 °C / Inert atmosphere
View Scheme
参考文献
Arias, Leire; Vara, Yosu; Cossio, Fernando P.
Journal of Organic Chemistry, 2012 , vol. 77, # 1 p. 266 - 275