2-(4-甲氧基苯基氨基)乙酸乙酯合成路线 （共 20 条）
反应条件
ammonium hydroxide in ethanol
参考文献
Glaxo Laboratories Limited
Patent: US3976680 A1, 1976 ;
反应条件
sodium hydroxide in methanol; water
13 h; Irradiation;
参考文献
Cantos, Albert; Marquet, Jorge; Moreno-Manas, Marcial; Gonzales-Lafont, Angels; Lluch, Jose M.; Bertran, Juan
Journal of Organic Chemistry, 1990 , vol. 55, # 10 p. 3303 - 3310
反应条件
water in ethanol
1 h; Ambient temperature;
参考文献
Gomaa, Mohsen Abdel-Motaal
Journal of Chemical Research - Part S, 1998 , # 10 p. 654 - 655
反应条件
1: molecular sieves 4 Angstroem / benzene / 20 °C
2: 95 percent / 2-propanol / [Ru(CO)2(Ph4C4CO)]2 / toluene; H2O / 1 h / 110 °C
View Scheme
参考文献
Samec, Joseph S.M.; Mony, Laetitia; Baeckvall, Jan-E.
Canadian Journal of Chemistry, 2005 , vol. 83, # 6-7 p. 909 - 916
反应条件
Ir(tetratolylporphyrinato)CH3 in dichloromethane
T=-78 - 22°C; Inert atmosphere;
参考文献
Anding, Bernie J.; Woo, L. Keith
Organometallics, 2013 , vol. 32, # 9 p. 2599 - 2607
反应条件
sulfuric acid in benzene
14 h; Heating;
参考文献
Hiremath; Biradar; Kudari
Journal of the Indian Chemical Society, 1984 , vol. 61, # 1 p. 74 - 76
反应条件
in diethyl ether
T=-50°C; 24 h;
参考文献
Saalfrank, Rolf W.; Weiss, Bernhard
Chemische Berichte, 1985 , vol. 118, # 7 p. 2626 - 2634
反应条件
in methanol; water
12 h; Irradiation;
参考文献
Cantos, Albert; Marquet, Jorge; Moreno-Manas, Marcial
Tetrahedron Letters, 1989 , vol. 30, # 18 p. 2423 - 2426
反应条件
1.1: lithium hydroxide hydrate / tetrahydrofuran; water / 2 h / 2 °C
1.2: 20 °C / pH 3 - 4
2.1: sodium nitrite / water / 0.33 h / 0 °C
3.1: acetic anhydride / 5 h / 100 °C
View Scheme
参考文献
Nithinchandra; Kalluraya; Aamir; Shabaraya
European Journal of Medicinal Chemistry, 2012 , vol. 54, p. 597 - 604
反应条件
1.1: lithium hydroxide hydrate / tetrahydrofuran; water / 2 h / 2 °C
1.2: 20 °C / pH 3 - 4
2.1: sodium nitrite / water / 0.33 h / 0 °C
View Scheme
参考文献
Fang, Yuesi; Wu, Chunrui; Larock, Richard C.; Shi, Feng
Journal of Organic Chemistry, 2011 , vol. 76, # 21 p. 8840 - 8851
