N-(5-甲氧基-2-甲基-苯基)乙酰胺合成路线 （共 16 条）
反应条件
1: 14.6 g / SnCl2*2H2O, conc. HCl / ethanol / 6 h / Heating
2: 10 g / pyridine / ethanol / 2 h / Heating
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参考文献
Karimov, A.; Telezhenetskaya, M. V.; Yunusov, S. Yu.
Chemistry of Natural Compounds, 1982 , vol. 18, # 4 p. 466 - 472
Khimiya Prirodnykh Soedinenii, 1982 , vol. 18, # 4 p. 498 - 504
参考文献
Kalle and Co.
Patent: DE239090 ;
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Friedlaender; Bruckner; Deutsch
Justus Liebigs Annalen der Chemie, 1912 , vol. 388, p. 34
Full Text Show Details
Kalle and Co.
Patent: DE232277 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 10, p. 468,485
反应条件
1.1: nitric acid; sulfuric acid / acetic acid / 3 h / 5 - 10 °C
2.1: potassium carbonate; acetic anhydride / chloroform; acetic acid / 40 °C
2.2: 60 °C
2.3: 2 h / 80 °C
3.1: hydrogenchloride; tin(ll) chloride / water / 4 h / 0 - 20 °C
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参考文献
Arora, Nidhi; Chen, Shaoqing; Hermann, Johannes Cornelius; Kuglstatter, Adreas; Labadie, Sharada Shenvi; Lin, Clara Jeou Jen; Lucas, Matthew C.; Moore, Amy Geraldine; Papp, Eva; Talamas, Francisco Xavier; Wanner, Jutta; Zhai, Yansheng
Patent: US2012/15962 A1, 2012 ;
US 20120015962 A1
反应条件
hydrogenchloride; potassium permanganate
1) water, heating; Yield given. Multistep reaction;
参考文献
Karimov, A.; Telezhenetskaya, M. V.; Yunusov, S. Yu.
Chemistry of Natural Compounds, 1982 , vol. 18, # 4 p. 466 - 472
Khimiya Prirodnykh Soedinenii, 1982 , vol. 18, # 4 p. 498 - 504
反应条件
oxygen; lithium chloride; copper dichloride in acetic acid
T=110°C; P=760.051 Torr; 24 h; regioselective reaction;
参考文献
Yang, Lujuan; Lu, Zhan; Stahl, Shannon S.
Chemical Communications, 2009 , # 42 p. 6460 - 6462
反应条件
sulfuryl dichloride in chloroform
参考文献
FMC Corporation
Patent: US5136868 A1, 1992 ;
