8,9-二甲氧基-6(5H)-菲啶酮合成路线 （共 6 条）
反应条件
palladium diacetate; sodium carbonate in N,N-dimethyl acetamide
T=160°C; 2.5 h;
参考文献
Rigby, James H.; Laurent, Stephane
Journal of Organic Chemistry, 1998 , vol. 63, # 19 p. 6742 - 6744
反应条件
phosphorus pentachloride
参考文献
Narasimhan, N. S.; Chandrachood, P. S.; Shete, N. R.
Tetrahedron, 1981 , vol. 37, p. 825 - 827
反应条件
in ethylene glycol dimethyl ether
T=180°C; Diels-Alder reaction; 120 h;
参考文献
Fujita, Reiko; Yoshisuji, Toshiteru; Wakayanagi, Sota; Wakamatsu, Hideaki; Matsuzaki, Hisao
Chemical and Pharmaceutical Bulletin, 2006 , vol. 54, # 2 p. 204 - 208
反应条件
1: trifluoromethylsulfonic anhydride; alpha-chloropyridine / dichloromethane / 0.33 h / -78 °C / |Inert atmosphere
2: boron trifluoride diethyl etherate / dichloromethane / 20 h / 20 °C
View Scheme
参考文献
In, Jinkyung; Hwang, Soonho; Kim, Changhun; Seo, Jae Hong; Kim, Sanghee
European Journal of Organic Chemistry, 2013 , # 5 p. 965 - 971
反应条件
in water; dimethyl sulfoxide
0.166667 h; Heating;
参考文献
Pereira, M. Manuela A.; Prabhakar, Sundaresan; Lobo, Ana M.
Journal of Natural Products, 1996 , vol. 59, # 8 p. 744 - 747
反应条件
1: 70 percent / aq. Na2CO3 / CHCl3 / 3 h
2: 60 percent / PCl5
View Scheme
参考文献
Narasimhan, N. S.; Chandrachood, P. S.; Shete, N. R.
Tetrahedron, 1981 , vol. 37, p. 825 - 827
