3-(氨基羰基)-1-苄基吡啶鎓氯化物合成路线 （共 23 条）
反应条件
1: 70 percent / 1-benzyl-1,4-dihydronicotinamide / acetonitrile; H2O / Ambient temperature
2: 1) 1-benzyl-1,4-dihydronicotinamide, 2) aq. HCl / 1) MeCN-H2O, room temp.
View Scheme
参考文献
Endo, Takeshi; Takada, Tadayoshi; Okawara, Makoto
Tetrahedron Letters, 1986 , vol. 27, # 5 p. 615 - 618
反应条件
1: 37 percent / methyl benzoylformate / acetonitrile; H2O / Ambient temperature
2: 1) 1-benzyl-1,4-dihydronicotinamide, 2) aq. HCl / 1) MeCN-H2O, room temp.
View Scheme
参考文献
Endo, Takeshi; Takada, Tadayoshi; Okawara, Makoto
Tetrahedron Letters, 1986 , vol. 27, # 5 p. 615 - 618
反应条件
1: ethanol / 40 °C
2: AgCl / water / 0.5 h
View Scheme
参考文献
Oppelt, Kerstin T.; Woess, Eva; Stiftinger, Martin; Schoefberger, Wolfgang; Buchberger, Wolfgang; Knoer, Guenther
Inorganic Chemistry, 2013 , vol. 52, # 20 p. 11910 - 11922
反应条件
1: ethanol / 40 °C
2: AgCl / water / 0.5 h
View Scheme
参考文献
Oppelt, Kerstin T.; Woess, Eva; Stiftinger, Martin; Schoefberger, Wolfgang; Buchberger, Wolfgang; Knoer, Guenther
Inorganic Chemistry, 2013 , vol. 52, # 20 p. 11910 - 11922
反应条件
AgCl in water
0.5 h;
参考文献
Oppelt, Kerstin T.; Woess, Eva; Stiftinger, Martin; Schoefberger, Wolfgang; Buchberger, Wolfgang; Knoer, Guenther
Inorganic Chemistry, 2013 , vol. 52, # 20 p. 11910 - 11922
反应条件
in acetonitrile
Mechanism;
参考文献
Miller, Larry L.; Valentine, James R.
Journal of the American Chemical Society, 1988 , vol. 110, # 12 p. 3982 - 3989
参考文献
Lettre et al.
Justus Liebigs Annalen der Chemie, 1953 , vol. 579, p. 123,130
Full Text Show Details
Schenley Ind.
Patent: US2697096 , 1950 ;
Full Text Show Details
Farbenfabr. Bayer
Patent: DE823594 , 1949 ;
DRP/DRBP Org.Chem.
反应条件
hydrogenchloride; NSC26899
1) MeCN-H2O, room temp.; Yield given. Multistep reaction;
参考文献
Endo, Takeshi; Takada, Tadayoshi; Okawara, Makoto
Tetrahedron Letters, 1986 , vol. 27, # 5 p. 615 - 618
反应条件
hydrogenchloride; NSC26899
1) MeCN-H2O, room temp.; Multistep reaction;
参考文献
Endo, Takeshi; Takada, Tadayoshi; Okawara, Makoto
Tetrahedron Letters, 1986 , vol. 27, # 5 p. 615 - 618
反应条件
in dichloromethane
51 h; Ambient temperatureother 1,4-dihydronicotinamide derivatives, var. solvent, presence and absence of Zn ion; Rate constantMechanism;
参考文献
Murakami, Yukito; Aoyama, Yasuhiro; Kikuchi, Jun-ichi
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 9 p. 2898 - 2901
