二氯化(环辛基-1,5-二烯)钌,聚合物合成路线 (共 4 条)
反应条件
in ethanol T=85°C; 5 h; Inert atmosphere;
参考文献
JSR Corporation
Patent: US2012/282414 A1, 2012 ;
Location in patent: Page/Page column 9 ;
反应条件
in tetrahydrofuran a mixt. of complex and aminophosphine was refluxed in THF under Ar for 6h, the mixt. was cooled to room temp.; the mixt. of isomers;
参考文献
Jia, Wenli; Chen, Xuanhua; Guo, Rongwei; Sui-Seng, Christine; Amoroso, Dino; Lough, Alan J.; Abdur-Rashid, Kamaluddin
Dalton Transactions, 2009 , # 39 p. 8301 - 8307
反应条件
in toluene a mixt. of complex and aminophosphine was refluxed in toluene under Ar for 6 h, the mixt. was cooled to room temp.; ether was added, suspn. was stirred for 1 h, filtered, washed with etherand dried under vac.; elem. anal.;
参考文献
Jia, Wenli; Chen, Xuanhua; Guo, Rongwei; Sui-Seng, Christine; Amoroso, Dino; Lough, Alan J.; Abdur-Rashid, Kamaluddin
Dalton Transactions, 2009 , # 39 p. 8301 - 8307
反应条件
in tetrahydrofuran a mixt. of complex and aminophosphine was refluxed in THF under Ar for 6h, the mixt. was cooled to room temp.; the mixt. of isomers;
参考文献
Jia, Wenli; Chen, Xuanhua; Guo, Rongwei; Sui-Seng, Christine; Amoroso, Dino; Lough, Alan J.; Abdur-Rashid, Kamaluddin
Dalton Transactions, 2009 , # 39 p. 8301 - 8307