7-(二乙基氨基)香豆素-3-羧酸合成路线 (共 15 条)
反应条件
UV-irradiation; Kinetics;
参考文献
Neveu, Pierre; Aujard, Isabelle; Benbrahim, Chouaha; Le Saux, Thomas; Allemand, Jean-Francois; Vriz, Sophie; Bensimon, David; Jullien, Ludovic
Angewandte Chemie - International Edition, 2008 , vol. 47, # 20 p. 3744 - 3746
反应条件
sulfuric acid 8 h; Heating;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 28, # 8 p. 872 - 880
Khimiya Geterotsiklicheskikh Soedinenii, , # 8 p. 1043 - 1052
反应条件
1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in dichloromethane T=20°C;
参考文献
Gustafson, Tiffany P.; Metzel, Greg A.; Kutateladze, Andrei G.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 13 p. 4752 - 4755
反应条件
silver carbonate; palladium dichloride in dimethyl sulfoxide
T=120°C; 5 h; Reagent/catalystSolventTemperature;
参考文献
Jafarpour, Farnaz; Zarei, Samaneh; Olia, Mina Barzegar Amiri; Jalalimanesh, Nafiseh; Rahiminejadan, Soraya
Journal of Organic Chemistry, 2013 , vol. 78, # 7 p. 2957 - 2964
反应条件
1: N,N-dimethyl-formamide With trichlorophosphate
T=40 - 50°C; 0.75 h;
2: 7-diethylaminocoumarin-3-carboxylic acid T=60°C; Vilsmeier Reaction; 2 h;
参考文献
An, Kyoung Lyong; Shin, Seung Rim; Jun, Kun; Park, Soo Youl
Journal of the Korean Chemical Society, 2014 , vol. 58, # 3 p. 297 - 302