1: N-[2-(tert-butyl-dimethyl-silanyloxy)-ethyl]-4-methyl-benzenesulfonamide With sodium hydride in tetrahydrofuran; mineral oil T=0 - 20°C; 1.5 h; Inert atmosphere; 2: methyl (2E,4E)-6-bromo-2,4-hexadienoate in tetrahydrofuran; mineral oil T=20°C; 20 h; Inert atmosphere; 3: With acetic acid in tetrahydrofuran; water T=20°C; 18 h; Inert atmosphere;
参考文献
Law, Katherine R.; McErlean, Christopher S. P.
Chemistry - A European Journal, 2013 , vol. 19, # 47 p. 15852 - 15855
N-bromosuccinmide; meta-chloroperoxybenzoic acid in chlorobenzene
1.5 h; Heating;
参考文献
Durrant, Graham; Green, Richard H.; Lambeth, Paul F.; Lester, Michael G.; Taylor, Nigel R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 2211 - 2214
