N-苄氧羰基-4-氨基丁酸合成路线 (共 42 条)
反应条件
methanol; Bacillus subtilis esterase in hexane T=37°C; pH=7.4; 0.5 h; aq. phosphate bufferEnzymatic reaction; Kinetics; Reagent/catalystTime;
参考文献
Barbayianni, Efrosini; Kokotos, Christoforos G.; Bartsch, Sebastian; Drakou, Christina; Bornscheuer, Uwe T.; Kokotos, George
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 14-15 p. 2325 - 2332
反应条件
methanol; Bacillus subtilis esterase in hexane T=37°C; pH=7.4; 0.5 h; aq. phosphate bufferEnzymatic reaction; Kinetics; Reagent/catalystTime;
参考文献
Barbayianni, Efrosini; Kokotos, Christoforos G.; Bartsch, Sebastian; Drakou, Christina; Bornscheuer, Uwe T.; Kokotos, George
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 14-15 p. 2325 - 2332
反应条件
ruthenium(IV) oxide; sodium periodate in tert-butyl alcohol T=20°C; 3 h;
参考文献
Kaname, Mamoru; Yoshifuji, Shigeyuki; Sashida, Haruki
Tetrahedron Letters, 2008 , vol. 49, # 17 p. 2786 - 2788
反应条件
methanol; Bacillus subtilis esterase in hexane T=37°C; pH=7.4; 0.5 h; aq. phosphate bufferEnzymatic reaction; Kinetics; Reagent/catalystTime;
参考文献
Barbayianni, Efrosini; Kokotos, Christoforos G.; Bartsch, Sebastian; Drakou, Christina; Bornscheuer, Uwe T.; Kokotos, George
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 14-15 p. 2325 - 2332
反应条件
water T=40 - 50°C; anschliessende Hydrierung an Raney-Nickel und Behandlung der Reaktionsloesung mit Chlorameisensaeure-benzylester und wss. NaOH unter Kuehlung;
参考文献
Hunt; du Vigneaud
Journal of Biological Chemistry, 1939 , vol. 127, p. 43,46
反应条件
1: triethylamine / tetrahydrofuran / 1 h 2: triethylamine / 1 h / 65 °C 3: sodium hydroxide / methanol / 1 h View Scheme
参考文献
Cal, Marta; Jaremko, Mariusz; Jaremko, Lukasz; Stefanowicz, Piotr
Amino Acids, 2013 , vol. 44, # 3 p. 1085 - 1091
反应条件
sodium hydroxide; benzyl chloroformate
参考文献
Winterstein et al.
Helvetica Chimica Acta, 1956 , vol. 39, p. 229,243
Full Text Show Details
Evans; Irreverre
Journal of Organic Chemistry, 1959 , vol. 24, p. 863
反应条件
1: triethylamine / 1 h / 65 °C 2: sodium hydroxide / methanol / 1 h View Scheme
参考文献
Cal, Marta; Jaremko, Mariusz; Jaremko, Lukasz; Stefanowicz, Piotr
Amino Acids, 2013 , vol. 44, # 3 p. 1085 - 1091
反应条件
1: triethylamine / 1 h / 65 °C 2: sodium hydroxide / methanol / 1 h View Scheme
参考文献
Cal, Marta; Jaremko, Mariusz; Jaremko, Lukasz; Stefanowicz, Piotr
Amino Acids, 2013 , vol. 44, # 3 p. 1085 - 1091
反应条件
phosphate buffer; Bacillus subtilis esterase BS2 in methanol; hexane T=37°C; pH=7.4; 1 h; Product distribution; Further Variations:reaction times; enzyme/substrate ratios;
参考文献
Fotakopoulou, Irene; Barbayianni, Efrosini; Constantinou-Kokotou, Violetta; Bornscheuer, Uwe T.; Kokotos, George
Journal of Organic Chemistry, 2007 , vol. 72, # 3 p. 782 - 786