2,4-二羟基-5-甲氧基苯甲醛合成路线 （共 18 条）
反应条件
potassium carbonate in acetone Etherification; 3 h; Heating;
参考文献
Mali, R. S.; Manekar, Anita R.; Tilve, S. G.
Organic Preparations and Procedures International, 1992 , vol. 24, # 1 p. 52 - 54
反应条件
Et2NC6H5 4 h; Heating;
参考文献
Maes, Dominick; Van Syngel, Kris; De Kimpe, Norbert
Heterocycles, 2008 , vol. 75, # 4 p. 1020 - 1021
反应条件
1: pyridine; aniline / 24 h / 20 °C 2: pyridine / ethylene glycol / Reflux View Scheme
参考文献
Cai, Xueting; Yang, Jie; Zhou, Jinpei; Lu, Wuguang; Hu, Chunping; Gu, Zhenhua; Huo, Jiege; Wang, Xiaoning; Cao, Peng
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 1 p. 84 - 92
反应条件
N,N-diethylaniline 4 h; Heating;
参考文献
Demyttenaere, Jan; Vervisch, Stijn; Debenedetti, Silvia; Coussio, Jorge; Maes, Dominick; De Kimpe, Norbert
Synthesis, 2004 , # 11 p. 1844 - 1848
参考文献
Chen, Lianqing; Yang, Chuluo; Li, Suyue; Qin, Jingui
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2007 , vol. 68, # 2 p. 317 - 322
反应条件
potassium carbonate; acetone
参考文献
Head; Robertson
Journal of the Chemical Society, 1931 , p. 1241,1244
反应条件
1: With AlCl3, aluminium chloride in dichloromethane
T=20°C; Reflux;
2: With hydrogenchloride in dichloromethane; water
参考文献
Cai, Xueting; Yang, Jie; Zhou, Jinpei; Lu, Wuguang; Hu, Chunping; Gu, Zhenhua; Huo, Jiege; Wang, Xiaoning; Cao, Peng
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 1 p. 84 - 92
反应条件
aluminium trichloride in dichloromethane
1 h; Ambient temperature;
参考文献
Mali, R. S.; Yadav, V. J.; Zaware, R. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, p. 759 - 760
反应条件
1: Br2; NaClO3
2: CuCl
View Scheme
参考文献
Chen, Lianqing; Yang, Chuluo; Li, Suyue; Qin, Jingui
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2007 , vol. 68, # 2 p. 317 - 322
反应条件
1: POCl3
2: Br2; NaClO3
3: CuCl
View Scheme
参考文献
Chen, Lianqing; Yang, Chuluo; Li, Suyue; Qin, Jingui
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2007 , vol. 68, # 2 p. 317 - 322
