1,2-硬脂酸甘油酯 甘油硬脂酸合成路线 （共 27 条）
反应条件
(i) Et3N, CHCl3, (ii) aq. KCl; Multistep reaction;
参考文献
Bogoslovskii,N.A. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1962 , vol. 32, # 7 p. 2210 - 2214,2177 - 2180
反应条件
1: (i) Et3N, (ii) Py, H2O View Scheme
参考文献
Nguyen Hoang Phuong et al.
Comptes Rendus des Seances de l'Academie des Sciences, Serie C: Sciences Chimiques, 1976 , vol. 283, p. 229 - 231
反应条件
(i) Et3N, CHCl3, (ii) aq. KCl, (iii) /BRN= 956566/; Multistep reaction;
参考文献
Eibl,H. et al.
Justus Liebigs Annalen der Chemie, 1967 , vol. 709, p. 226 - 230
反应条件
ethanol; lipase from Rhizopus Delemar immobilized on EP100 in hexane
T=40°C; 48 h; Product distribution / selectivity;
参考文献
DIVERSA CORPORATION
Patent: WO2005/32496 A2, 2005 ;
Location in patent: Page/Page column 227; 18/138 ;
参考文献
Senju Pharmaceutical Co., Ltd.
Patent: US5098898 A1, 1992 ;
反应条件
T=200°C; 36 h; Inert atmosphere;
参考文献
Sutter, Marc; Dayoub, Wissam; Metay, Estelle; Raoul, Yann; Lemaire, Marc
Green Chemistry, 2013 , vol. 15, # 3 p. 786 - 797
反应条件
sulfuric acid
T=70°C;
参考文献
Gruen; Corelli
Angewandte Chemie, 1912 , vol. 25, p. 667
参考文献
Renshaw
Journal of the American Chemical Society, 1914 , vol. 36, p. 540
Full Text Show Details
Guth
Zeitschrift fuer Biologie (Munich), vol. 44, p. 86
反应条件
pyridinium p-toluenesulfonate in ethanol
参考文献
Lie Ken Jie, Marcel S.F.; Lam
Chemistry and Physics of Lipids, 1995 , vol. 77, # 2 p. 155 - 171
反应条件
1: pyridinium p-toluenesulfonate / CH2Cl2
2: KMnO4, acetic anhydride / H2O
3: 1.) DCC, DMAP / 1.) CH2Cl2, 2.) CH2Cl2
4: PPTS / ethanol
View Scheme
参考文献
Lie Ken Jie, Marcel S.F.; Lam
Chemistry and Physics of Lipids, 1995 , vol. 77, # 2 p. 155 - 171
