1,2-硬脂酸甘油酯 甘油硬脂酸合成路线 （共 27 条）
反应条件
1: 1.) DCC, DMAP / 1.) CH2Cl2, 2.) CH2Cl2
2: PPTS / ethanol
View Scheme
参考文献
Lie Ken Jie, Marcel S.F.; Lam
Chemistry and Physics of Lipids, 1995 , vol. 77, # 2 p. 155 - 171
反应条件
1: KMnO4, acetic anhydride / H2O
2: 1.) DCC, DMAP / 1.) CH2Cl2, 2.) CH2Cl2
3: PPTS / ethanol
View Scheme
参考文献
Lie Ken Jie, Marcel S.F.; Lam
Chemistry and Physics of Lipids, 1995 , vol. 77, # 2 p. 155 - 171
参考文献
Gruen
Collegium, 1927 , p. 3
反应条件
HMS-TBD in dimethyl sulfoxide
T=110°C; 4 h;
参考文献
Kharchafi, Ghizlane; Jerome, Francois; Adam, Isabelle; Pouilloux, Yannick; Barrault, Joel
New Journal of Chemistry, 2005 , vol. 29, # 7 p. 928 - 934
反应条件
sodium methylate
T=115°C; 4 h;
参考文献
Adlof, Richard O.; List, Gary R.
Journal of Agricultural and Food Chemistry, 2003 , vol. 51, # 7 p. 2096 - 2099
反应条件
T=200°C; im luftverduennten Raum;
参考文献
Kreis; Hafner
Chemische Berichte, 1903 , vol. 36, p. 1124
Full Text Show Details
Ulzer; Batik; Sommer
Patent: DE189839 ;
反应条件
lipozyme RM IM
T=65°C; Enzymatic reactionneat (no solvent); regioselective reaction;
参考文献
Fernandes, Jane Luiza Nogueira; De Souza, Rodrigo Octavio Mendonca Alves; De Vasconcellos Azeredo, Rodrigo Bagueira
Magnetic Resonance in Chemistry, 2012 , vol. 50, # 6 p. 424 - 428
反应条件
T=70°C; 12 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bhati, Asharam; Hamilton, Richard J.; Steven, David A.; Aneja, Rajender; Padley, Frederick B.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , # 10 p. 1553 - 1558
反应条件
T=70°C; 12 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bhati, Asharam; Hamilton, Richard J.; Steven, David A.; Aneja, Rajender; Padley, Frederick B.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , # 10 p. 1553 - 1558
反应条件
T=70°C; 12 h; in dark; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bhati, Asharam; Hamilton, Richard J.; Steven, David A.; Aneja, Rajender; Padley, Frederick B.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , # 10 p. 1553 - 1558
