1,2-硬脂酸甘油酯 甘油硬脂酸合成路线 （共 27 条）
反应条件
1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine
T=110°C; 6 h; other guanine-catalysts; var. reaction times; Product distribution;
参考文献
Guimaraes Aguiar, Leila M.; Vargas, Rogerio Matheus
JAOCS, Journal of the American Oil Chemists' Society, 1998 , vol. 75, # 6 p. 755 - 756
反应条件
1: 1.5 h / 120 °C / atmosphere of dry argon
2: 1.5 h / 120 °C / atmosphere of dry argon
3: iodosylbenzene / benzene / 1 h / 18 - 20 °C
4: NaI / acetone / 1.5 h / Heating
5: KRS-40T resin in H+ form / CHCl3; methanol; H2O / 0.25 h / 18 - 20 °C
6: 42 percent / H2 / palladium black / CHCl3; methanol / 1 h
View Scheme
参考文献
Smirnova, L.I.; Malenkovskaya, M. A.; Predvoditelev, D. A.; Nifant'ev, E. E.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, p. 1011 - 1019
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 6 p. 1170 - 1179
反应条件
1: (i) Et3N, (ii) Py, H2O
View Scheme
参考文献
Nguyen Hoang Phuong et al.
Comptes Rendus des Seances de l'Academie des Sciences, Serie C: Sciences Chimiques, 1976 , vol. 283, p. 229 - 231
反应条件
(i) Et3N, CHCl3, (ii) aq. KCl, (iii) /BRN= 956566/; Multistep reaction;
参考文献
Eibl,H. et al.
Justus Liebigs Annalen der Chemie, 1967 , vol. 709, p. 226 - 230
反应条件
1: 1-methyl-imidazole
2: Zn, TsOH, Py
3: 2,4,6-triisopropylbenzenesulfonyl chloride, Py
4: H2 / Pd-C
5: isopentyl nitrite, Py, AcOH
View Scheme
参考文献
Lammers,J.G.; van Boom,J.H.
Recueil des Travaux Chimiques des Pays-Bas, 1979 , vol. 98, p. 243 - 250
反应条件
1: (i) Et3N, (ii) Py, H2O
View Scheme
参考文献
Nguyen Hoang Phuong et al.
Comptes Rendus des Seances de l'Academie des Sciences, Serie C: Sciences Chimiques, 1976 , vol. 283, p. 229 - 231
反应条件
(i) Et3N, CHCl3, (ii) aq. KCl, (iii) /BRN= 956566/; Multistep reaction;
参考文献
Eibl,H. et al.
Justus Liebigs Annalen der Chemie, 1967 , vol. 709, p. 226 - 230
