1-(4-甲氧基苄基)-3,4,5,6,7,8,-六氢异喹啉合成路线 （共 6 条）
反应条件
1: pyridine; tetrahydrofuran / 8 h / 0 °C 2: H2 / Ru(OCOCF3)2<(S)-tolbinap> / methanol / 100 h / 30 °C / 76000.1 Torr View Scheme
参考文献
Kitamura, M.; Hsiao, Yi; Noyori, R.; Takaya, H.
Tetrahedron Letters, 1987 , vol. 28, # 41 p. 4829 - 4832
反应条件
1: pyridine; tetrahydrofuran / 8 h / 0 °C 2: H2 / Ru(OCOCF3)2<(S)-tolbinap> / methanol / 100 h / 30 °C / 76000.1 Torr View Scheme
参考文献
Kitamura, M.; Hsiao, Yi; Noyori, R.; Takaya, H.
Tetrahedron Letters, 1987 , vol. 28, # 41 p. 4829 - 4832
反应条件
aluminium trichloride; sodium iodide in acetonitrile
T=20°C; 3.2 h;
参考文献
Konwar, Dilip; Boruah, Monalisa; Sarmah, Gautom Kumar; Bhattacharyya, Nayan Kamal; Borthakur, Naleen; Goswami, Birendra Nath; Boruah, Kumar Ranjan
Journal of Chemical Research - Part S, 2001 , # 11 p. 490 - 492
反应条件
1: 5 h / 150 °C
2: POCl3 / benzene / Heating
View Scheme
参考文献
Kitamura, M.; Hsiao, Yi; Noyori, R.; Takaya, H.
Tetrahedron Letters, 1987 , vol. 28, # 41 p. 4829 - 4832
反应条件
1: 5 h / 150 °C
2: POCl3 / benzene / Heating
View Scheme
参考文献
Kitamura, M.; Hsiao, Yi; Noyori, R.; Takaya, H.
Tetrahedron Letters, 1987 , vol. 28, # 41 p. 4829 - 4832
反应条件
1: pyridine / tetrahydrofuran / 8 h / 0 °C
2: H2 / Ru(CF3COO)2<(R)-TolBINAP> / methanol / 164 h / 30 °C / 76000 Torr
View Scheme
参考文献
Kitamura, M.; Hsiao, Yi; Noyori, R.; Takaya, H.
Tetrahedron Letters, 1987 , vol. 28, # 41 p. 4829 - 4832
