2-溴-4,5-二甲氧基苯磺酰氯合成路线 （共 5 条）
参考文献
Levi; Smiles
Journal of the Chemical Society, 1931 , p. 520,525
反应条件
chlorosulfonic acid
T=0°C; 0.583333 h;
参考文献
Evans, Paul; McCabe, Thomas; Morgan, Ben S.; Reau, Sophie
Organic Letters, 2005 , vol. 7, # 1 p. 43 - 46
反应条件
triethylamine in dichloromethane
T=0 - 20°C; 15 h;
参考文献
Evans, Paul; McCabe, Thomas; Morgan, Ben S.; Reau, Sophie
Organic Letters, 2005 , vol. 7, # 1 p. 43 - 46
反应条件
1: 87 percent / triethylamine / CH2Cl2 / 15 h / 0 - 20 °C
2: 83 percent / di(tricyclohexylphosphine)(benzylidene)ruthenium dichloride / CH2Cl2 / 24 h / 20 °C
View Scheme
参考文献
Evans, Paul; McCabe, Thomas; Morgan, Ben S.; Reau, Sophie
Organic Letters, 2005 , vol. 7, # 1 p. 43 - 46
反应条件
1: 93 percent / triethylamine / CH2Cl2 / 15 h / 0 - 20 °C
2: 61 percent / Pd(OAc)2; triphenylphosphine; K2CO3 / dimethylformamide / 18 h / 110 °C
View Scheme
参考文献
Evans, Paul; McCabe, Thomas; Morgan, Ben S.; Reau, Sophie
Organic Letters, 2005 , vol. 7, # 1 p. 43 - 46
