反应条件
1.1: N,N,N',N'-tetramethylethylenediamine; n-butyllithium / tetrahydrofuran; hexane / 0.67 h / -78 °C 1.2: N,N,N',N'-tetramethylethylenediamine; O2 / hexane; tetrahydrofuran / 7 h / 20 °C 2.1: 83 percent / sodium borohydride / 2-methyl-propan-2-ol / 1 h / Heating 3.1: 72 percent / oxalyl chloride; DMSO; triethylamine / CH2Cl2 / -60 - 20 °C View Scheme
参考文献
Baptistella, Lucia H. B.; Aleixo, Adriana M.
Synthetic Communications, 2002 , vol. 32, # 19 p. 2937 - 2950
