(S)-(+)-2-苄氨基-1-苯乙醇合成路线 （共 33 条）
反应条件
sodium tetrahydroborate in methanol 0.5 h; Ambient temperature;
参考文献
Alcaide, Benito; Escobar, Gerardo; Perez-Ossorio, Rafael; Plumet, Joaquin; Sanz, Dionisia
Journal of Chemical Research, Miniprint, 1984 , # 5 p. 1466 - 1488
反应条件
lithium aluminium tetrahydride
参考文献
Gaylord; Kay
Journal of the American Chemical Society, 1956 , vol. 78, p. 2167
反应条件
1: 1 M DIBALH / diethyl ether; hexane / 3 h / -80 °C 2: diethyl ether; hexane; methanol / 1.5 h / Ambient temperature 3: NaBH4 / diethyl ether; hexane; methanol / Ambient temperature 4: 93 percent / LiAlH4 / tetrahydrofuran / 1 h / Heating View Scheme
参考文献
Vries, Erik F. J. de; Brussee, Johannes; Gen, Arne van der
Journal of Organic Chemistry, 1994 , vol. 59, # 23 p. 7133 - 7137
反应条件
1: NaBH4 / diethyl ether; hexane; methanol / Ambient temperature 2: 93 percent / LiAlH4 / tetrahydrofuran / 1 h / Heating View Scheme
参考文献
Vries, Erik F. J. de; Brussee, Johannes; Gen, Arne van der
Journal of Organic Chemistry, 1994 , vol. 59, # 23 p. 7133 - 7137
反应条件
1: 81 percent / bis<(1,1'-diphenylphosphino)ferrocene>palladium(II) chloride / diethyl ether / 16 h / Ambient temperature 2: 95 percent / LiAlH4 / tetrahydrofuran / 4 h / Heating View Scheme
参考文献
Pridgen, Lendon N.; Killmer, Lewis B.; Webb, R. Lee
Journal of Organic Chemistry, 1982 , vol. 47, # 11 p. 1985 - 1989
反应条件
1: 95 percent / CH3ONa / methanol / 16 h / 20 °C 2: 81 percent / bis<(1,1'-diphenylphosphino)ferrocene>palladium(II) chloride / diethyl ether / 16 h / Ambient temperature 3: 95 percent / LiAlH4 / tetrahydrofuran / 4 h / Heating View Scheme
参考文献
Pridgen, Lendon N.; Killmer, Lewis B.; Webb, R. Lee
Journal of Organic Chemistry, 1982 , vol. 47, # 11 p. 1985 - 1989
反应条件
lithium aluminium tetrahydride
参考文献
Kawamoto; Wills
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 16 p. 1916 - 1928
反应条件
1: 100 percent / tetrabutylammonium fluoride / tetrahydrofuran / 48 h / Ambient temperature 2: 70 percent / NaBH4 / methanol / 0.17 h View Scheme
参考文献
Tsuge, Otohiko; Kanemasa, Shuji; Hatada, Akira; Matsuda, Koyo
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, p. 2537 - 2546
反应条件
1.1: sodium tetrahydroborate / ethanol / 0.5 h 1.2: 0.25 h 2.1: sodium tetrahydroborate / tetrahydrofuran; ethanol / 0.5 h View Scheme
参考文献
Ayala-Mata, Francisco; Barrera-Mendoza, Citlalli; Jimenez-Vazquez, Hugo A.; Vargas-Diaz, Elena; Zepeda, L. Gerardo
Molecules, 2012 , vol. 17, # 12 p. 13864 - 13878
反应条件
1: 100 percent / tetrabutylammonium fluoride / tetrahydrofuran / 48 h / Ambient temperature 2: 70 percent / NaBH4 / methanol / 0.17 h View Scheme
参考文献
Tsuge, Otohiko; Kanemasa, Shuji; Hatada, Akira; Matsuda, Koyo
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, p. 2537 - 2546
