2-氯-N,2-二苯基乙酰胺合成路线 （共 14 条）
反应条件
1: chloroform; N-benzylideneaniline With sodium hydroxide
T=20°C; 0.5 h; AutoclaveGreen chemistry;
2: carbon dioxide T=100°C; P=15001.5 Torr; 5 h; Green chemistry;
参考文献
Song, Qing-Wen; Yu, Bing; Liu, An-Hua; He, Ying; Yang, Zhen-Zhen; Diao, Zhen-Feng; Song, Qing-Chuan; Li, Xue-Dong; He, Liang-Nian
RSC Advances, 2013 , vol. 3, # 41 p. 19009 - 19014
反应条件
triethylamine; phenyl N-phenylphosphoroamidochloridate in dichloromethane
0.5 h; Ambient temperature;
参考文献
Mestres, Ramon; Palomo, Claudio
Synthesis, 1982 , # 4 p. 288 - 291
反应条件
sodium hydroxide in diethyl ether
0 deg C, 1 h, then r.t., 1.5 h;
参考文献
Aoyama; Nakano; Marumo; Uno; Shioiri
Synthesis, 1991 , # 12 p. 1163 - 1167
反应条件
sulfuric acid in acetic anhydride; acetic acid
T=0°C; 2 h;
参考文献
Khlebnikov, A. F.; Kostikov, R. R.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1984 , vol. 20, # 7 p. 739 - 744
Khimiya Geterotsiklicheskikh Soedinenii, 1984 , vol. 20, # 7 p. 912 - 916
反应条件
sulfuric acid in acetic acid
T=0°C; 2 h;
参考文献
Khlebnikov, A. F.; Kostikov, R. R.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1984 , vol. 20, # 7 p. 739 - 744
Khimiya Geterotsiklicheskikh Soedinenii, 1984 , vol. 20, # 7 p. 912 - 916
反应条件
1.1: ethanol
2.1: sodium hydroxide / 0.5 h / 20 °C / |Autoclave; |Green chemistry
2.2: 5 h / 100 °C / 15001.5 Torr / |Green chemistry
View Scheme
参考文献
Song, Qing-Wen; Yu, Bing; Liu, An-Hua; He, Ying; Yang, Zhen-Zhen; Diao, Zhen-Feng; Song, Qing-Chuan; Li, Xue-Dong; He, Liang-Nian
RSC Advances, 2013 , vol. 3, # 41 p. 19009 - 19014
反应条件
1.1: ethanol
2.1: sodium hydroxide / 0.5 h / 20 °C / |Autoclave; |Green chemistry
2.2: 5 h / 100 °C / 15001.5 Torr / |Green chemistry
View Scheme
参考文献
Song, Qing-Wen; Yu, Bing; Liu, An-Hua; He, Ying; Yang, Zhen-Zhen; Diao, Zhen-Feng; Song, Qing-Chuan; Li, Xue-Dong; He, Liang-Nian
RSC Advances, 2013 , vol. 3, # 41 p. 19009 - 19014
反应条件
in ethylene glycol dimethyl ether
18 h; Heating;
参考文献
Busby, Reginald E.; Khan, Mohammad A.; Khan, Mohammad R.; Parrick, John; Shaw, C. J. Granville
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1431 - 1435
反应条件
phosphorus pentachloride
参考文献
Bischoff; Walden
Justus Liebigs Annalen der Chemie, 1894 , vol. 279, p. 123
参考文献
Kostikov,R.R. et al.
Zhurnal Organicheskoi Khimii, 1977 , vol. 13, # 9 p. 1857 - 1871,1721 - 1733
