反应条件
1: 1.) 2-methyl-2-propyllithium, 2.) I2 / 1.) pentane, THF, -78 deg C, 1 h, 2.) THF, RT, 72 h 2: 12 percent / tetrakis(triphenylphosphine)palladium / tetrahydrofuran / -78 deg C,then RT, 5 days View Scheme
参考文献
Barbero, Nekane; Martin, Ruben
Organic Letters, 2012 , vol. 14, # 3 p. 796 - 799