反应条件
1: 1.) Mg, I2 / 1.) THF, reflux, 30 min, 2.) THF, reflux, 2 h
2: 50 percent / sulfuric acid, H2O / 1.5 h / 100 °C
3: 99 percent / benzene; diethyl ether / 16 h / Heating
4: TiCl3, LiAlH4 / tetrahydrofuran / 2 h / Heating
5: 83 percent / Fermy's salt, KH2PO4, H2O / benzene / 0.5 h
6: 94 percent / NaBH4, O2 / ethanol / 72 h
7: m-chlorobenzoic acid / tetrahydrofuran / 0.5 h / Ambient temperature
View Scheme
参考文献
Lee; Harvey
Journal of Organic Chemistry, 1986 , vol. 51, # 18 p. 3502 - 3507
