反应条件
1.1: sodium hypochlorite; acetic acid / water / 3.33 h / 0 - 17 °C / |Large scale
2.1: acetic acid / n-heptane / 3 h / 40 - 90 °C / |Large scale
3.1: n-hexyl lithium / tetrahydrofuran; hexane / 2 h / -50 - 50 °C / |Large scale
3.2: 0.58 h / -25 - -5 °C / |Large scale
4.1: hydrogenchloride; water / 1.5 h / 50 °C / |Large scale
View Scheme
参考文献
Scott, Jeremy P.; Ashwood, Michael S.; Brands, Karel M. J.; Brewer, Sarah E.; Cowden, Cameron J.; Dolling, Uif-H.; Emerson, Khateeta M.; Gibb, Andrew D.; Goodyear, Adrian; Oliver, Steven F.; Stewart, Gavin W.; Wallace, Debra J.
Organic Process Research and Development, 2008 , vol. 12, # 4 p. 723 - 730
