芴甲氧羰基-(R)-3-氨基-3-(2-萘基)-丙酸合成路线 (共 2 条)
反应条件
1: (R)-3,3'-bis(3,5-bis(trifluoromethyl)phenyl)-1,1'-binaphthyl-2,2'-disulfonimide / chloroform / 240 h / 18 °C 2: osmium(VIII) oxide; sodium periodate / tetrahydrofuran; water; tert-butyl alcohol / 4 h / 20 °C 3: 2-methyl-but-2-ene; sodium chlorite; sodium dihydrogenphosphate / water; tert-butyl alcohol / 12 h / 20 °C View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 9 p. 2573 - 2576
Angew. Chem., , vol. 125, # 9 p. 2633 - 2636,4
反应条件
1: (R)-3,3'-bis(3,5-bis(trifluoromethyl)phenyl)-1,1'-binaphthyl-2,2'-disulfonimide / chloroform / 240 h / 18 °C 2: osmium(VIII) oxide; sodium periodate / tetrahydrofuran; water; tert-butyl alcohol / 4 h / 20 °C 3: 2-methyl-but-2-ene; sodium chlorite; sodium dihydrogenphosphate / water; tert-butyl alcohol / 12 h / 20 °C View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 9 p. 2573 - 2576
Angew. Chem., , vol. 125, # 9 p. 2633 - 2636,4