N-甲基哌啶-3-羧酰胺盐酸盐合成路线 （共 4 条）
反应条件
hydrogen; palladium 10 on activated carbon in ethyl acetate
T=20°C; 2 h;
参考文献
QUONOVA LLC
Patent: WO2009/77844 A2, 2009 ;
Location in patent: Page/Page column 67 ;
反应条件
potassium hydroxide; nickel monoaluminide
21.2 h; Heating;
参考文献
Lunn, George; Sansone, Eric B.
Journal of Organic Chemistry, 1986 , vol. 51, # 4 p. 513 - 517
反应条件
trifluoroacetic acid in dichloromethane
参考文献
Baek, Bong-Hyeon; Lee, Myung-Ryul; Kim, Kwang-Yon; Cho, Ung-In; Boo, Doo Wan; Shin, Injae
Tetrahedron Letters, 2003 , vol. 44, # 17 p. 3447 - 3450
反应条件
1: benzotriazole-1-yl-oxy-tris(dimethylamino)phosphonium*PF6(1-; N-hydroxybenzotriazole (HOBt); DIEA
2: 30 percent TFA / CH2Cl2
View Scheme
参考文献
Baek, Bong-Hyeon; Lee, Myung-Ryul; Kim, Kwang-Yon; Cho, Ung-In; Boo, Doo Wan; Shin, Injae
Tetrahedron Letters, 2003 , vol. 44, # 17 p. 3447 - 3450
