5-(4-甲基苯基)5-苯基乙内酰脲合成路线 (共 6 条)
反应条件
potassium hydroxide in ethanol T=40°C; 2 h; Ultrasound irradiation;
参考文献
Ultrasonics Sonochemistry, , vol. 17, # 1 p. 55 - 57
反应条件
potassium hydroxide in ethanol; water T=20°C; 0.0666667 h; Sonication;
参考文献
Chinese Journal of Chemistry, , vol. 28, # 2 p. 255 - 258
反应条件
anhydrous ammonium carbonate in various solvent(s) modified Bucherer-Bergs reaction; Heating;
参考文献
Journal of Heterocyclic Chemistry, , vol. 37, # 4 p. 773 - 777
反应条件
1: bromine / CHCl3 2: 77 percent / DMSO / 4 h / 100 - 120 °C 3: 71 percent / 40 percent aq. NaOH / ethanol; H2O / 3 h / Heating; 13C-labelling; other ureas, other benzils View Scheme
参考文献
Archiv der Pharmazie, , vol. 326, # 1 p. 45 - 50
反应条件
1: 77 percent / DMSO / 4 h / 100 - 120 °C 2: 71 percent / 40 percent aq. NaOH / ethanol; H2O / 3 h / Heating; 13C-labelling; other ureas, other benzils View Scheme
参考文献
Archiv der Pharmazie, , vol. 326, # 1 p. 45 - 50
反应条件
1: AlCl3 / 0 to 25 deg C, 1-2 h 2: bromine / CHCl3 3: 77 percent / DMSO / 4 h / 100 - 120 °C 4: 71 percent / 40 percent aq. NaOH / ethanol; H2O / 3 h / Heating; 13C-labelling; other ureas, other benzils View Scheme
参考文献
Archiv der Pharmazie, , vol. 326, # 1 p. 45 - 50