1: With lithium aluminium tetrahydride in diethyl ether
T=20°C; 24 h; Inert atmosphere;
2: With sulfuric acid; water in diethyl ether
Cooling with ice;
参考文献
Hekking, Koen F. W.; Waalboer, Dennis C. J.; Moelands, Marcel A. H.; Van Delft, Floris L.; Rutjes, Floris P. J. T.
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 1 p. 95 - 106
lithium aluminium tetrahydride in tetrahydrofuran
T=0°C; 1 h;
参考文献
Bromidge, Steven M.; Sammes, Peter G.; Street, Leslie J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1725 - 1730