反应条件
1: 90 percent / Zn, AcOH / H2O / 0.25 h / Heating
2: 1.) SOCl2 / 1.) CHCl3, reflux, 40 min, 2.) CHCl3, 2 h, reflux
3: 1.) NaH, 2.) copper oxide, NaI / 1.) dioxane, 1h, reflux, 2.) dioxane, 6 h, reflux
View Scheme
参考文献
Binder, Dieter; Prager, Bernhard C.; Noe, Christian R.
Journal of Chemical Research, Miniprint, 1981 , # 5 p. 1801 - 1824
