1-氯-4-(乙基硫代)苯合成路线 （共 23 条）
反应条件
aluminium trichloride in carbon disulfide
3 h; Heating;
参考文献
Abdel-Wahab, Aboel-Magd A.; El-Khawaga, Ahmed M.; El-Zohry, Maher F.; Khalaf, Ali A.
Phosphorus and Sulfur and the Related Elements, 1984 , vol. 19, p. 31 - 44
反应条件
1: 81 percent / Et3N / toluene / 3 h / Ambient temperature
2: 600 °C / 0 - 0.1 Torr
View Scheme
参考文献
Aitken, R. Alan; Armstrong, Jill M.; Drysdale, Martin J.; Ross, Fiona C.; Ryan, Bruce M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1999 , # 5 p. 593 - 604
反应条件
1: 72 percent / CH2Cl2
2: 85 percent / 0.36 M sodium ethoxide / ethanol
View Scheme
参考文献
Bird, Roger; Griffiths, Gwerydd; Griffiths, Gwynfor F.; Stirling, Charles J. M.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1982 , p. 579 - 584
反应条件
in N,N-dimethyl-formamide; acetone
Reflux;
参考文献
Salomon, Pierre; Zard, Samir Z.
Organic Letters, 2014 , vol. 16, # 5 p. 1482 - 1485
反应条件
T=600°C; P=0.001 - 0.1 Torr; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Aitken, R. Alan; Armstrong, Jill M.; Drysdale, Martin J.; Ross, Fiona C.; Ryan, Bruce M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1999 , # 5 p. 593 - 604
反应条件
sulfuric acid in carbon disulfide
40 h; Ambient temperature;
参考文献
El-Khawaga, A. M.; El-Zohry, M. F.; Ismail, M. T.; Abdel-Wahab, A. A.; Khalaf, A. A.
Phosphorus and Sulfur and the Related Elements, 1987 , vol. 29, p. 265 - 270
反应条件
1: 85 percent / hexamethylphosphoric acid triamide / 0.5 h / 100 °C
2: 30 percent / hexamethylphosphoric acid triamide / 1 h / 120 °C
View Scheme
参考文献
Chianelli, Donatella; Testaferri, Lorenzo; Tiecco, Marcello; Tingoli, Marco
Synthesis, 1982 , # 6 p. 475 - 478
反应条件
1: 72 percent / Et3N
2: 1 percent / 0 h / 500 - 600 °C / 0.01 Torr
View Scheme
参考文献
Aitken, R. Alan; Drysdale, Martin J.; Ryan, Bruce M.
Journal of the Chemical Society, Chemical Communications, 1994 , # 7 p. 805 - 806
参考文献
Shostakovskii,M.F. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1960 , vol. 30, # 4 p. 1123 - 1130,1141 - 1147
参考文献
Olivato, Paulo R.; Guerrero, Sandra A.; Martins, Elizabeth A. L.
Phosphorus, Sulfur and Silicon and the Related Elements, 1989 , vol. 44, p. 9 - 16
