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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-联苯硼酸
合成路线
（共 120 条）
719-98-2
+
5122-94-1
4-联苯硼酸
→
反应条件
177551-63-2
4-三氟甲基磺酰基联苯
反应条件
[2,2']bipyridinyl; potassium carbonate; copper(l) chloride in ethylene glycol dimethyl ether T=45°C; 18 h; Schlenk techniqueInert atmosphereSealed tube;
参考文献
Pluta, Roman; Nikolaienko, Pavlo; Rueping, Magnus
Angewandte Chemie - International Edition, 2014 , vol. 53, # 6 p. 1650 - 1653
Angew. Chem., 2014 , vol. 126, # 6 p. 1676 - 1679,4
5122-94-1
4-联苯硼酸
+
81290-20-2
(三氟甲基)三甲基硅烷
→
反应条件
177551-63-2
4-三氟甲基磺酰基联苯
反应条件
potassium phosphate; 1,10-phenanthroline; copper(I) isothiocyanate; sulfur; silver carbonate in N,N-dimethyl-formamide T=20°C; 24 h; Molecular sieveInert atmosphere;
参考文献
Chen, Chao; Xie, Yan; Chu, Lingling; Wang, Ruo-Wen; Zhang, Xingang; Qing, Feng-Ling
Angewandte Chemie - International Edition, 2012 , vol. 51, # 10 p. 2492 - 2495
→
反应条件
177551-63-2
4-三氟甲基磺酰基联苯
反应条件
[2,2']bipyridinyl; [Cu(I)(CH3CN)4]PF6; potassium carbonate in diethylene glycol dimethyl ether T=35°C; 15 h; Schlenk techniqueInert atmosphere; Reagent/catalystSolvent;
参考文献
Shao, Xinxin; Wang, Xueqiang; Yang, Tao; Lu, Long; Shen, Qilong
Angewandte Chemie - International Edition, 2013 , vol. 52, # 12 p. 3457 - 3460
Angew. Chem., 2013 , vol. 125, # 12 p. 3541 - 3544,4
5122-94-1
4-联苯硼酸
+
65-85-0
苯甲酸
→
反应条件
2170-13-0
4-二苯基苯甲酸
反应条件
[bis(acetoxy)iodo]benzene; triethylamine; 1,1'-carbonyldiimidazole in dichloromethane T=20°C; 3 h;
参考文献
Ruso, Jayaraman Sembian; Rajendiran, Nagappan; Kumaran, Rajendran Senthil
Tetrahedron Letters, 2014 , vol. 55, # 15 p. 2345 - 2347
5122-94-1
4-联苯硼酸
+
98-88-4
苯甲酰氯
→
反应条件
2170-13-0
4-二苯基苯甲酸
反应条件
oxygen; cesium fluoride; bis[2-(diphenylphosphino)phenyl] ether; bis(dibenzylideneacetone)-palladium(0) in anhydrous xylene T=60°C; P=760.051 Torr; 12 h;
参考文献
Chen, Jiuxi; Peng, Yong; Liu, Miaochang; Ding, Jinchang; Su, Weike; Wu, Huayue
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 11-12 p. 2117 - 2122
589-87-7
对溴碘苯
+
5122-94-1
4-联苯硼酸
→
反应条件
1762-84-1
4-溴对三联苯
反应条件
1: 4-bromo-1-iodobenzene With tetrakis(triphenylphosphine) palladium(0) in ethylene glycol dimethyl ether T=20°C; 0.166667 h; 2: 1,1'-Biphenyl-4-yl-boronic acid With sodium carbonate in ethylene glycol dimethyl ether 12 h; Heating; Further stages.;
参考文献
Dingemans, Theo J.; Murthy, N. Sanjeeva; Samulski, Edward T.
Journal of Physical Chemistry B, 2001 , vol. 105, # 37 p. 8845 - 8860
5122-94-1
4-联苯硼酸
+
65-85-0
苯甲酸
→
反应条件
2128-93-0
4-苯基二苯甲酮
反应条件
1: benzoic acid With potassium phosphate in 1,4-dioxane T=20°C; 0.0833333 h; Inert atmosphere; 2: With DMEG in 1,4-dioxane T=20°C; 2 h; Inert atmosphere; 3: 1,1'-Biphenyl-4-yl-boronic acid With tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=90°C; 16 h; Inert atmosphereSealed tube;
参考文献
Pathak, Arunendra; Rajput, Chatrasal S.; Bora, Pushkar S.; Sharma, Somesh
Tetrahedron Letters, 2013 , vol. 54, # 17 p. 2149 - 2150
7334-48-7
+
5122-94-1
4-联苯硼酸
→
反应条件
2128-93-0
4-苯基二苯甲酮
反应条件
sodium carbonate; triphenylphosphine; palladium diacetate in toluene T=100°C; Suzuki cross-coupling; 12 h;
参考文献
Lim, Kyoung-Chan; Hong, Young-Taek; Kim, Sunggak
Synlett, 2006 , # 12 p. 1851 - 1854
5122-94-1
4-联苯硼酸
+
106-95-6
3-溴丙烯
→
反应条件
20120-35-8
反应条件
tris-(dibenzylideneacetone)dipalladium(0); potassium carbonate in toluene T=110°C; Suzuki-Miyaura coupling; 15 h; Inert atmosphere;
参考文献
Gerbino, Dario C.; Mandolesi, Sandra D.; Schmalz, Hans-Guenther; Podesta, Julio C.
European Journal of Organic Chemistry, 2009 , # 23 p. 3964 - 3972
17135-74-9
1,8-二溴萘
+
5122-94-1
4-联苯硼酸
+
98-80-6
→
反应条件
反应条件
1: 1,8-dibromo-naphthalene; 3,4,5-trimethoxyphenylboronic acid With palladium diacetate; potassium carbonate in water; N,N-dimethyl-formamide T=100°C; Suzuki-Miyaura cross-coupling; 3 h; 2: 1,1'-Biphenyl-4-yl-boronic acid With palladium diacetate; potassium carbonate in water; N,N-dimethyl-formamide T=100°C; Suzuki-Miyaura cross-coupling; 4 h;
参考文献
Lima, Carlos F.R.A.C.; Rodriguez-Borges, Jose E.; Santos, Luis M.N.B.F.
Tetrahedron, 2011 , vol. 67, # 4 p. 689 - 697
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