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乙二醇
甲醛
63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-联苯硼酸
合成路线
（共 120 条）
17135-74-9
1,8-二溴萘
+
5122-94-1
4-联苯硼酸
+
98-80-6
苯硼酸
→
反应条件
反应条件
1: 1,8-dibromo-naphthalene; 1,1'-Biphenyl-4-yl-boronic acid With palladium diacetate; potassium carbonate in water; N,N-dimethyl-formamide T=100°C; Suzuki-Miyaura cross-coupling; 3 h; 2: 3,4,5-trimethoxyphenylboronic acid With palladium diacetate; potassium carbonate in water; N,N-dimethyl-formamide T=100°C; Suzuki-Miyaura cross-coupling; 4 h;
参考文献
Lima, Carlos F.R.A.C.; Rodriguez-Borges, Jose E.; Santos, Luis M.N.B.F.
Tetrahedron, 2011 , vol. 67, # 4 p. 689 - 697
2052-07-5
2-溴联苯
+
5122-94-1
4-联苯硼酸
→
反应条件
1165-58-8
1-苯基-2-(4-苯基苯基)苯
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in water; N,N-dimethyl-formamide T=0°C; Suzuki-Miyaura Coupling; 5 h; Inert atmosphere;
参考文献
Lima, Carlos F. R. A. C.; Rodrigues, Ana S. M. C.; Silva, Vera L. M.; Silva, Artur M. S.; Santos, Luis M. N. B. F.
ChemCatChem, 2014 , vol. 6, # 5 p. 1291 - 1302
273-53-0
苯并恶唑
+
5122-94-1
4-联苯硼酸
→
反应条件
17064-45-8
2-联苯苯并噁唑
反应条件
potassium phosphate; 1,10-phenanthroline; copper diacetate; palladium diacetate in dimethyl sulfoxide T=80°C; 24 h;
参考文献
Ranjit, Sadananda; Liu, Xiaogang
Chemistry - A European Journal, 2011 , vol. 17, # 4 p. 1105 - 1108
106-38-7
对溴甲苯
+
5122-94-1
4-联苯硼酸
→
反应条件
28952-41-2
反应条件
caesium carbonate; bis(η3-allyl-μ-chloropalladium(II)) in 1,4-dioxane T=90°C; Suzuki-Miyaura cross-coupling reaction; 15 h;
参考文献
Kuriyama, Masami; Shimazawa, Rumiko; Shirai, Ryuichi
Tetrahedron, 2007 , vol. 63, # 38 p. 9393 - 9400
624-31-7
4-碘甲苯
+
5122-94-1
4-联苯硼酸
→
反应条件
28952-41-2
反应条件
[Ru(η4-COD)(η3-methylallyl)2]; sodium t-butanolate in CPME; water T=60°C; Suzuki-Miyaura coupling; 12 h; Inert atmosphere;
参考文献
Kawatsura, Motoi; Kamesaki, Kosuke; Yamamoto, Mitsuaki; Hayase, Shuichi; Itoh, Toshiyuki
Chemistry Letters, 2010 , vol. 39, # 10 p. 1050 - 1051
5122-94-1
4-联苯硼酸
→
反应条件
28952-41-2
反应条件
1: 68 percent / Pd(PPh3)4; Na2CO3 / H2O; toluene; ethanol / 6 h / Heating 2: 86 percent / dppeNiCl2 / tetrahydrofuran; diethyl ether / 12 h / Heating View Scheme
参考文献
Cho, Chul-Hee; Sun, Myungchul; Seo, Yong-Seok; Kim, Chul-Bae; Park, Kwangyong
Journal of Organic Chemistry, 2005 , vol. 70, # 4 p. 1482 - 1485
5122-94-1
4-联苯硼酸
+
96898-10-1
→
反应条件
71274-84-5
4-三氟甲氧基联苯
反应条件
1: 1,1'-Biphenyl-4-yl-boronic acid With sodium hydroxide in methanol T=23°C; 0.25 h; Inert atmosphere; 2: With AgPF6 in methanol T=0°C; 0.5 h; Inert atmosphere; 3: tris(dimethylamino)sulfonium trifluoromethoxide Further stages;
参考文献
Huang, Chenghong; Liang, Theresa; Harada, Shinji; Lee, Eunsung; Ritter, Tobias
Journal of the American Chemical Society, 2011 , vol. 133, # 34 p. 13308 - 13310
1666-13-3
二苯基二硒醚
+
5122-94-1
4-联苯硼酸
→
反应条件
65490-22-4
反应条件
1: With 1,10-phenanthroline; copper(II) sulfate in ethanol 0.0166667 h; Schlenk technique; 2: With sodium carbonate in ethanol T=20°C; 5 h; Schlenk technique;
参考文献
Zheng, Bo; Gong, Ying; Xu, Hua-Jian
Tetrahedron, 2013 , vol. 69, # 26 p. 5342 - 5347
5122-94-1
4-联苯硼酸
+
74628-02-7
→
反应条件
67035-92-1
反应条件
sodium carbonate; triphenylphosphine; palladium diacetate in tetrahydrofuran T=60°C; Suzuki cross-coupling; 12 h;
参考文献
Lim, Kyoung-Chan; Hong, Young-Taek; Kim, Sunggak
Synlett, 2006 , # 12 p. 1851 - 1854
95-16-9
苯并噻唑
+
5122-94-1
4-联苯硼酸
→
反应条件
67362-98-5
反应条件
potassium phosphate; 1,10-phenanthroline; copper diacetate; palladium diacetate in dimethyl sulfoxide T=80°C; 24 h;
参考文献
Ranjit, Sadananda; Liu, Xiaogang
Chemistry - A European Journal, 2011 , vol. 17, # 4 p. 1105 - 1108
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