2-[(4-甲氧基苯甲酰基)氨基]乙酸乙酯合成路线 （共 12 条）
反应条件
copper(l) iodide; calcium carbonate in water; acetonitrile T=40°C; 6 h;
参考文献
Yoo, Woo-Jin; Li, Chao-Jun
Journal of the American Chemical Society, 2006 , vol. 128, # 40 p. 13064 - 13065
反应条件
tert.-butylhydroperoxide; copper(l) iodide; silver(I) iodate; calcium carbonate in water; acetonitrile T=40°C; 6 h;
参考文献
Giguere-Bisson, Maxime; Yoo, Woo-Jin; Li, Chao-Jun
Organic Syntheses, 2012 , vol. 88, p. 14 - 21
反应条件
water; sodium acetate in acetonitrile T=0°C; 1.16667 h; Inert atmosphere;
参考文献
Basavanag, Unnamatla M. V.; Dos Santos, Aurelie; El Kaim, Laurent; Gamez-Montano, Rocio; Grimaud, Laurence
Angewandte Chemie - International Edition, 2013 , vol. 52, # 28 p. 7194 - 7197
Angew. Chem., 2013 , vol. 125, # 28 p. 7335 - 7338,4
反应条件
triethylamine in 1,4-dioxane 0.166667 h; Ambient temperature;
参考文献
Theocharis, A.B.; Maroulis, A.J.; Hadjiantoniou-Maroulis, C.P.; Alexandrou, N.E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 619 - 621
参考文献
Munakata; Tanaka; Toyoshima
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 7 p. 2045 - 2051
反应条件
1: SOCl2, DMF / toluene / 0.5 h / 60 - 70 °C 2: K2CO3 / H2O; toluene / -5 - 5 °C View Scheme
参考文献
Munakata; Tanaka; Toyoshima
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 7 p. 2045 - 2051
反应条件
1: methanol / Ambient temperature 2: 48 percent / lead tetra-acetate / CH2Cl2; acetic acid / 0.5 h / 0 °C 3: 97 percent / triethylamine / dioxane / 0.17 h / Ambient temperature View Scheme
参考文献
Theocharis, A.B.; Maroulis, A.J.; Hadjiantoniou-Maroulis, C.P.; Alexandrou, N.E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 619 - 621
反应条件
1: 48 percent / lead tetra-acetate / CH2Cl2; acetic acid / 0.5 h / 0 °C 2: 97 percent / triethylamine / dioxane / 0.17 h / Ambient temperature View Scheme
参考文献
Theocharis, A.B.; Maroulis, A.J.; Hadjiantoniou-Maroulis, C.P.; Alexandrou, N.E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 619 - 621
反应条件
potassium hydroxide; phosphate buffer; μ = 1.0; anhydrous tetramethylammonium chloride in 1,4-dioxane; water T=25°C; var. pH; Rate constantMechanism;
参考文献
Cline, Gary W.; Hanna, Samir B.
Journal of Organic Chemistry, 1988 , vol. 53, # 15 p. 3583 - 3586
反应条件
1,1'-carbonyldiimidazole 1) DMF, 0 deg C -> room temperature, 20 min, 2) DMF, room temperature, 30 min; Yield given. Multistep reaction;
参考文献
Conway, Samuel C.; Perni, Robert B.
Synthetic Communications, 1998 , vol. 28, # 9 p. 1539 - 1545
