1-(4-(溴甲基)苯基)乙酮合成路线 （共 16 条）
反应条件
in 1,4-dioxane; water T=90°C; 2 h;
参考文献
Pieck, J. Carsten; Kuch, David; Grolle, Friederike; Linne, Uwe; Haas, Clemens; Carell, Thomas
Journal of the American Chemical Society, 2006 , vol. 128, # 5 p. 1404 - 1405
反应条件
1: potassium tert-butylate / ethanol; tert-butyl alcohol / 24 h / Inert atmosphere; Reflux 2: hydrogenchloride / 1,4-dioxane / 8 h / Reflux View Scheme
参考文献
Satyanarayana, Maragani; Vitali, Francesca; Frost, John R.; Fasan, Rudi
Chemical Communications, 2012 , vol. 48, # 10 p. 1461 - 1463
反应条件
1: sodium azide; acetic acid / ethanol; water / 74 h / 4 °C 2: chloroform / Photolysis View Scheme
参考文献
Ranaweera, Ranaweera A. A. Upul; Zhao, Yu; Muthukrishnan, Sivaramakrishnan; Keller, Christopher; Gudmundsdottir, Anna D.
Australian Journal of Chemistry, 2010 , vol. 63, # 12 p. 1645 - 1655
反应条件
diisopropylamine in tetrahydrofuran T=80°C; sealed tube;
参考文献
JACKSON, Paul Francis; Leonard, Kristi Anne; Barbay, Joseph Kent; Wang, Aihua; Tounge, Brett Andrew; Zhang, Yan; Maharoof, Umar S.M.
Patent: US2012/302569 A1, 2012 ;
Location in patent: Page/Page column 34 ;
反应条件
1: potassium tert-butylate / ethanol; tert-butyl alcohol / 24 h / Inert atmosphere; Reflux 2: hydrogenchloride / 1,4-dioxane / 8 h / Reflux View Scheme
参考文献
Satyanarayana, Maragani; Vitali, Francesca; Frost, John R.; Fasan, Rudi
Chemical Communications, 2012 , vol. 48, # 10 p. 1461 - 1463
反应条件
1: benzene / 72 h / Heating
2: NaOCH3 / methanol; benzene
View Scheme
参考文献
Pandey, Saurabh; Srivastava
Indian Journal of Chemistry - Section A Inorganic, Physical, Theoretical and Analytical Chemistry, 2002 , vol. 41, # 2 p. 333 - 338
