5,5-二甲基-2-苯基-1,3,2-二氧硼杂合成路线 （共 155 条）
反应条件
magnesium sulfate in diethyl ether T=25°C; 20 h; Inert atmosphere;
参考文献
Matthew, Smitha C.; Glasspoole, Ben W.; Eisenberger, Patrick; Crudden, Cathleen M.
Journal of the American Chemical Society, 2014 , vol. 136, # 16 p. 5828 - 5831
反应条件
in tetrahydrofuran T=20°C; 2 h; Inert atmosphere;
参考文献
Myslinska, Malgorzata; Heise, Glenn L.; Walsh, Dana J.
Tetrahedron Letters, 2012 , vol. 53, # 24 p. 2937 - 2941
反应条件
1: 3-hydroxy-2,2-dimethylpropanol With tetrakis(dimethylamino)diboron; potassium acetate in tetrahydrofuran T=80°C; 0.5 h; 2: trifluoromethanesulfonyloxybenzene With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; triphenylphosphine in tetrahydrofuran T=80°C; 22 h;
参考文献
BASF SE; SCHMIDT-LEITHOFF, Joachim; PICHLMAIR, Stefan; BELLO, Charles; BASF (CHINA) COMPANY LIMITED
Patent: WO2013/14579 A1, 2013 ;
Location in patent: Page/Page column 15; 16 ;
反应条件
1: tri-phenyl-antimony With boron trichloride in dichloromethane T=0°C; 2 h; 2: With methanol T=20°C; 0.5 h; 3: 3-hydroxy-2,2-dimethylpropanol in methanol T=20°C; 1 h;
参考文献
Yasuike, Shuji; Nakata, Kazuhide; Qin, Weiwei; Kaji, Toshiyuki; Kurita, Jyoji
Chemistry Letters, 2006 , vol. 35, # 12 p. 1402 - 1403
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; [1,3-bis(diphenylphosphino) propane] dichloronickel(II); triethylamine; zinc in toluene T=100°C; 2 h; Inert atmosphere;
参考文献
Wilson, Daniela A.; Wilson, Christopher J.; Moldoveanu, Costel; Resmerita, Ana-Maria; Corcoran, Patrick; Hoang, Lisa M.; Rosen, Brad M.; Percec, Virgil
Journal of the American Chemical Society, 2010 , vol. 132, # 6 p. 1800 - 1801
反应条件
potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in dimethyl sulfoxide T=80°C; 3 h;
参考文献
Bello, Charles S.; Schmidt-Leithoff, Joachim
Tetrahedron Letters, 2012 , vol. 53, # 46 p. 6230 - 6235,6
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; [1,3-bis(diphenylphosphino) propane] dichloronickel(II); triethylamine; zinc in toluene T=100°C; 2 h; Inert atmosphere;
参考文献
Wilson, Daniela A.; Wilson, Christopher J.; Moldoveanu, Costel; Resmerita, Ana-Maria; Corcoran, Patrick; Hoang, Lisa M.; Rosen, Brad M.; Percec, Virgil
Journal of the American Chemical Society, 2010 , vol. 132, # 6 p. 1800 - 1801
反应条件
[RhCl(cod)]2; Xantphos; DABCO in toluene 100°C, 15 h;
参考文献
Tobisu, Mamoru; Kinuta, Hirotaka; Kita, Yusuke; Remond, Emmanuelle; Chatani, Naoto
Journal of the American Chemical Society, 2012 , vol. 134, # 1 p. 115 - 118
反应条件
1: Ph2SbCl With boron trichloride in dichloromethane T=0°C; 2 h; 2: With methanol T=20°C; 0.5 h; 3: 3-hydroxy-2,2-dimethylpropanol in methanol T=20°C; 1 h;
参考文献
Yasuike, Shuji; Nakata, Kazuhide; Qin, Weiwei; Kaji, Toshiyuki; Kurita, Jyoji
Chemistry Letters, 2006 , vol. 35, # 12 p. 1402 - 1403
反应条件
Ni(PCy3)2Cl2; sodium t-butanolate; tri-cyclo-hexyl-phosphine in ethylene glycol dimethyl ether; toluene T=110°C; 24 h; Inert atmosphere;
参考文献
Huang, Kun; Yu, Da-Gang; Zheng, Shu-Fang; Wu, Zhen-Hua; Shi, Zhang-Jie
Chemistry - A European Journal, 2011 , vol. 17, # 3 p. 786 - 791
