5,5-二甲基-2-苯基-1,3,2-二氧硼杂合成路线 （共 155 条）
反应条件
oxygen; copper(l) chloride; lithium tert-butylate in N,N-dimethyl-formamide T=40°C; P=760.051 Torr; 0.166667 h;
参考文献
Chemistry - A European Journal, , vol. 17, # 23 p. 6321 - 6325
反应条件
oxygen; copper(l) chloride; lithium tert-butylate in N,N-dimethyl-formamide T=40°C; P=760.051 Torr; 0.166667 h;
参考文献
Yang, Fanzhi; Xu, Zhaoqing; Wang, Zhe; Yu, Zhengkun; Wang, Rui
Chemistry - A European Journal, 2011 , vol. 17, # 23 p. 6321 - 6325
反应条件
(+/-)-SynPhos; palladium diacetate; triethylamine T=40°C; P=760.051 Torr; 24 h;
参考文献
Angewandte Chemie - International Edition, , vol. 49, # 19 p. 3371 - 3374
反应条件
bis(1,5-cyclooctadiene)nickel (0); potassium phosphate; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; 12 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Resmerita, Ana-Maria; Rosen, Brad M.; Percec, Virgil
Journal of Organic Chemistry, 2011 , vol. 76, # 24 p. 9946 - 9955
反应条件
C39H32OP2*CuCl; sodium t-butanolate in toluene T=80°C; Suzuki-Miyaura Coupling; 15 h; Inert atmosphereGlovebox;
参考文献
Zhou, Yiqing; You, Wei; Smith, Kevin B.; Brown, M. Kevin
Angewandte Chemie - International Edition, 2014 , vol. 53, # 13 p. 3475 - 3479
Angew. Chem., 2014 , vol. 126, # 13 p. 3543 - 3547,5
反应条件
sodium hydroxide; tetrabutylammomium bromide; palladium on activated charcoal T=100°C; Suzuki-Miyaura cross-coupling; 2 h;
参考文献
Lysen, Morten; Koehler, Klaus
Synthesis, 2006 , # 4 p. 692 - 698
反应条件
palladium diacetate; caesium carbonate in methanol; toluene T=60°C; Suzuki coupling; 4 h;
参考文献
Myslinska, Malgorzata; Heise, Glenn L.; Walsh, Dana J.
Tetrahedron Letters, 2012 , vol. 53, # 24 p. 2937 - 2941
反应条件
bis(1,5-cyclooctadiene)nickel (0); potassium phosphate; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; 12 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 76, # 24 p. 9946 - 9955
反应条件
bis(1,2-diphenylphosphino)benzene; copper (II) acetate monohydrate; lithium tert-butylate in tetrahydrofuran T=20°C; Chan-Lam type coupling; 4 h; Inert atmosphere;
参考文献
Matsuda, Naoki; Hirano, Koji; Satoh, Tetsuya; Miura, Masahiro
Angewandte Chemie - International Edition, 2012 , vol. 51, # 15 p. 3642 - 3645
反应条件
bis(1,5-cyclooctadiene)nickel (0); cesium fluoride; tri-cyclo-hexyl-phosphine in toluene T=120°C; Suzuki-Miyaura coupling; 12 h;
参考文献
Tobisu, Mamoru; Shimasaki, Toshiaki; Chatani, Naoto
Angewandte Chemie - International Edition, 2008 , vol. 47, # 26 p. 4866 - 4869
