2-脱氧-1-乙酸-3,5-二苯甲酸-D-赤式-五呋喃糖合成路线 (共 6 条)
反应条件
1: 95 percent / KI, dibenzo-18-crown-6 / acetonitrile; toluene / Heating; time: 2 - 4h 2: 38 percent / NH3 / methanol View Scheme
参考文献
Tetrahedron Letters, , vol. 31, # 31 p. 4437 - 4440
反应条件
1: 77 percent / KI, dibenzo-18-crown-6 / acetonitrile; toluene / Heating 2: 46 percent / NH3 / methanol View Scheme
参考文献
Baud; Chavis; Lucas; Imbach
Tetrahedron Letters, 1990 , vol. 31, # 31 p. 4437 - 4440
反应条件
1: 95 percent / KI, dibenzo-18-crown-6 / acetonitrile; toluene / Heating; time: 2 - 4h 2: 62 percent / NH3 / methanol View Scheme
参考文献
Baud; Chavis; Lucas; Imbach
Tetrahedron Letters, 1990 , vol. 31, # 31 p. 4437 - 4440
反应条件
1: 31 percent / trimethylsilyl trifluoromethanesulfonate / acetonitrile / 1.3 h / Ambient temperature 2: 67 percent / ammonia / methanol / 15 h / 40 °C View Scheme
参考文献
Yamaguchi; Saneyoshi
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 4 p. 1441 - 1450
反应条件
sulfuric acid; acetic acid
参考文献
Rubira, Maria-Jose; Perez-Perez, Maria-Jesus; Balzarini, Jan; Camarasa, Maria-Jose
Synlett, 1998 , # 2 p. 177 - 179
反应条件
pyridine
Ambient temperature; Yield given;
参考文献
Baud; Chavis; Lucas; Imbach
Tetrahedron Letters, 1990 , vol. 31, # 31 p. 4437 - 4440