甲基-2-脱氧-alpha-D-呋喃核糖苷合成路线 (共 3 条)
反应条件
hydrogenchloride in diethyl ether T=20°C; Product distribution / selectivity;
参考文献
JOHNSON MATTHEW PUBLIC LIMITED COMPANY; FU, Xing; ZUMBRUNN, Albercht
Patent: WO2012/71508 A1, 2012 ;
Location in patent: Page/Page column 5-6; 8 ;
反应条件
1: methanol With acetyl chloride T=20°C; Inert atmosphere; 2: 2-deoxy-D-arabinopyranose T=20°C; Inert atmosphere;
参考文献
Ludek, Olaf R.; Marquez, Victor E.
Tetrahedron, 2009 , vol. 65, # 41 p. 8461 - 8467
反应条件
hydrogenchloride 15 h; Ambient temperature; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Jandu; Selwood
Journal of Organic Chemistry, 1995 , vol. 60, # 16 p. 5170 - 5173