(4-甲酰基-2-甲氧基)苯氧基乙酸乙酯合成路线 (共 6 条)
反应条件
potassium carbonate in acetone 4 h; RefluxInert atmosphere;
参考文献
Nagaraju, Manda; Chandra, Rajesh; Gawali, Bhimrao B.
Synlett, 2012 , vol. 23, # 10 art. no. ST-2012-D0241-L, p. 1485 - 1488
参考文献
Biorex Laboratories Limited
Patent: US4190671 A1, 1980 ;
反应条件
CuCl2·2H2O; water in acetonitrile T=75°C; 1.5 h;
参考文献
Quan, Na; Shi, Xiao-Xin; Nie, Liang-Deng; Dong, Jing; Zhu, Rui-Heng
Synlett, 2011 , # 7 p. 1028 - 1032
反应条件
alum in neat (no solvent) T=80°C; 12 h; Green chemistry;
参考文献
Shunmugadhas, Ganesan; Kumar, Suresh; Kumaresan, Sudalaiandi
Journal of Chemical Sciences (Bangalore), 2012 , vol. 124, # 4 p. 857 - 863,7
反应条件
1: With sodium hydroxide in tetrahydrofuran; methanol; water T=20°C; 33 h; 2: With hydrogenchloride in tetrahydrofuran; methanol; water pH=3;
参考文献
Ki Choi, Seok; Thomas, Thommey; Li, Ming-Hsin; Kotlyar, Alina; Desai, Ankur; Baker Jr., James R.
Chemical Communications, 2010 , vol. 46, # 15 p. 2632 - 2634
反应条件
1: sodium hydroxide / water; methanol; tetrahydrofuran / 20 °C
2: nitric acid / acetic acid / 0 - 20 °C
View Scheme
参考文献
Inlay, Matthew A.; Choe, Veronica; Bharathi, Sophia; Fernhoff, Nathaniel B.; Baker, James R.; Weissman, Irving L.; Choi, Seok Ki
Chemical Communications, 2013 , vol. 49, # 43 p. 4971 - 4973