5-羟基-4',7-二甲氧基黄酮合成路线 （共 39 条）
反应条件
sodium carbonate in N,N-dimethyl-formamide T=20°C; 12 h; Inert atmosphere;
参考文献
Lu, Kui; Chu, Jie; Wang, Haomeng; Fu, Xiaoli; Quan, Dewu; Ding, Hongxia; Yao, Qingwei; Yu, Peng
Tetrahedron Letters, 2013 , vol. 54, # 47 p. 6345 - 6348
反应条件
boron tribromide in dichloromethane 5 h; Ambient temperature;
参考文献
Zembower, David E.; Zhang, Heping
Journal of Organic Chemistry, 1998 , vol. 63, # 25 p. 9300 - 9305
反应条件
potassium carbonate in N,N-dimethyl-formamide T=20°C;
参考文献
Quintin, Jerome; Lewin, Guy
Journal of Natural Products, 2004 , vol. 67, # 9 p. 1624 - 1627
反应条件
in methanol; diethyl ether T=20°C; 0.5 h;
参考文献
Matsuda, Hisashi; Morikawa, Toshio; Toguchida, Iwao; Yoshikawa, Masayuki
Chemical and Pharmaceutical Bulletin, 2002 , vol. 50, # 6 p. 788 - 795
反应条件
potassium hydroxide in water; acetone T=20°C; 4 h;
参考文献
Kou, Li-Qun; Cheng, Xin-Li; Zhang, Zun-Ting
Journal of Chemical Crystallography, 2008 , vol. 38, # 1 p. 21 - 25
反应条件
4-methylmorpholine N-oxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in dimethyl sulfoxide T=20°C; 48 h;
参考文献
Righi, Giuliana; Silvestri, Ilaria Proietti; Barontini, Maurizio; Crisante, Fernanda; Di Manno, Andrea; Pelagalli, Romina; Bovicelli, Paolo
Natural Product Research, 2012 , vol. 26, # 14 p. 1278 - 1284
反应条件
1: 68 percent / HCOONH4 / Pd/C / methanol / 2.5 h / Heating 2: 95 percent / K2CO3 / dimethylformamide / 20 °C View Scheme
参考文献
Quintin, Jerome; Lewin, Guy
Journal of Natural Products, 2004 , vol. 67, # 9 p. 1624 - 1627
反应条件
1: 53 percent / HCOONH4 / Pd/C / methanol / 5 h / Heating 2: 70 percent / aq. HCl / 1.5 h / 50 - 55 °C 3: 95 percent / K2CO3 / dimethylformamide / 20 °C View Scheme
参考文献
Quintin, Jerome; Lewin, Guy
Journal of Natural Products, 2004 , vol. 67, # 9 p. 1624 - 1627
反应条件
1: 66 percent / KHCO3 / dimethylformamide / 2.5 h / 120 °C 2: 67 percent / KHCO3 / dimethylformamide / 1 h / 120 °C 3: 68 percent / HCOONH4 / Pd/C / methanol / 2.5 h / Heating 4: 95 percent / K2CO3 / dimethylformamide / 20 °C View Scheme
参考文献
Quintin, Jerome; Lewin, Guy
Journal of Natural Products, 2004 , vol. 67, # 9 p. 1624 - 1627
反应条件
1: 40 percent / KHCO3 / dimethylformamide / 2 h / 80 °C 2: 53 percent / HCOONH4 / Pd/C / methanol / 5 h / Heating 3: 70 percent / aq. HCl / 1.5 h / 50 - 55 °C 4: 95 percent / K2CO3 / dimethylformamide / 20 °C View Scheme
参考文献
Quintin, Jerome; Lewin, Guy
Journal of Natural Products, 2004 , vol. 67, # 9 p. 1624 - 1627
