5-羟基-4',7-二甲氧基黄酮合成路线 （共 39 条）
反应条件
1: 67 percent / KHCO3 / dimethylformamide / 1 h / 120 °C 2: 68 percent / HCOONH4 / Pd/C / methanol / 2.5 h / Heating 3: 95 percent / K2CO3 / dimethylformamide / 20 °C View Scheme
参考文献
Quintin, Jerome; Lewin, Guy
Journal of Natural Products, 2004 , vol. 67, # 9 p. 1624 - 1627
反应条件
in methanol; hexane; dichloromethane T=20°C; 12 h;
参考文献
Sasaki, Hiroaki; Kitoh, Yuki; Miki, Kazuhiko; Kinoshita, Kaoru; Koyama, Kiyotaka; Kaneda, Miyuki; Takahashi, Kunio
Heterocycles, 2012 , vol. 85, # 11 p. 2749 - 2756
反应条件
potassium carbonate; acetone
参考文献
Hasegawa; Shirato
Journal of the American Chemical Society, 1952 , vol. 74, p. 6114
Journal of the American Chemical Society, 1955 , vol. 77, p. 3557
反应条件
1: 81.4 percent / pyridine / 0.17 h / 100 °C 2: 69.1 percent / KOH / pyridine / 0.17 h / 100 °C 3: 70.8 percent / H2SO4 / acetic acid / 0.17 h / 100 °C 4: 85.4 percent / BBr3 / CH2Cl2 / 5 h / Ambient temperature View Scheme
参考文献
Zembower, David E.; Zhang, Heping
Journal of Organic Chemistry, 1998 , vol. 63, # 25 p. 9300 - 9305
反应条件
1: 69.1 percent / KOH / pyridine / 0.17 h / 100 °C 2: 70.8 percent / H2SO4 / acetic acid / 0.17 h / 100 °C 3: 85.4 percent / BBr3 / CH2Cl2 / 5 h / Ambient temperature View Scheme
参考文献
Zembower, David E.; Zhang, Heping
Journal of Organic Chemistry, 1998 , vol. 63, # 25 p. 9300 - 9305
反应条件
1: 70.8 percent / H2SO4 / acetic acid / 0.17 h / 100 °C 2: 85.4 percent / BBr3 / CH2Cl2 / 5 h / Ambient temperature View Scheme
参考文献
Zembower, David E.; Zhang, Heping
Journal of Organic Chemistry, 1998 , vol. 63, # 25 p. 9300 - 9305
反应条件
1: 81.4 percent / pyridine / 0.17 h / 100 °C 2: 69.1 percent / KOH / pyridine / 0.17 h / 100 °C 3: 70.8 percent / H2SO4 / acetic acid / 0.17 h / 100 °C 4: 85.4 percent / BBr3 / CH2Cl2 / 5 h / Ambient temperature View Scheme
参考文献
Zembower, David E.; Zhang, Heping
Journal of Organic Chemistry, 1998 , vol. 63, # 25 p. 9300 - 9305
反应条件
pyridine; iodine 8 h; Heating;
参考文献
Lee, Yean-Jang; Wu, Tsao-Dong
Journal of the Chinese Chemical Society, 2001 , vol. 48, # 2 p. 201 - 206
反应条件
1: 70 percent / aq. HCl / 1.5 h / 50 - 55 °C 2: 95 percent / K2CO3 / dimethylformamide / 20 °C View Scheme
参考文献
Quintin, Jerome; Lewin, Guy
Journal of Natural Products, 2004 , vol. 67, # 9 p. 1624 - 1627
反应条件
methanol; potassium hydroxide
参考文献
Coulerie, Paul; Nour, Mohammed; Maciuk, Alexandre; Eydoux, Cecilia; Guillemot, Jean-Claude; Lebouvier, Nicolas; Hnawia, Edouard; Leblanc, Karine; Lewin, Guy; Canard, Bruno; Figadere, Bruno
Planta Medica, 2013 , vol. 79, # 14 p. 1313 - 1318
