5-氯-2-硝基苯甲酸甲酯合成路线 （共 26 条）
反应条件
potassium carbonate in N,N-dimethyl-formamide T=40°C; 1 h;
参考文献
STATE OF OREGON ACTING BY AND THROUGH THE STATE BOARD OF HIGHER EDUCATION ON BEHALF OF OREGON STATE UNIVERSITY
Patent: WO2008/156656 A2, 2008 ;
Location in patent: Page/Page column 44; 179-180 ;
反应条件
potassium carbonate in acetone Esterification; 0.5 h; Heating;
参考文献
Kondo, Kazumi; Ogawa, Hidenori; Yamashita, Hiroshi; Miyamoto, Hisashi; Tanaka, Michinori; Nakaya, Kenji; Kitano, Kazuyoshi; Yamamura, Yoshitaka; Nakamura, Shigeki; Onogawa, Toshiyuki; Mori, Toyoki; Tominaga, Michiaki
Bioorganic and Medicinal Chemistry, 1999 , vol. 7, # 8 p. 1743 - 1754
反应条件
thionyl chloride T=0°C; 15 h; Heating / reflux;
参考文献
KIRIN BEER KABUSHIKI KAISHA
Patent: EP1614676 A1, 2006 ;
Location in patent: Page/Page column 161 ;
EP 1614676 A1
参考文献
Rohm and Haas Company
Patent: US4259510 A1, 1981 ;
反应条件
in methanol; dichloromethane
参考文献
Merck and Co., Inc.; E. I. Du Pont De Nemours and Co.
Patent: US5256667 A1, 1993 ;
US 5256667 A
反应条件
in acetonitrile T=30°C; KineticsThermodynamic data;
参考文献
Kondo, Yasuhiko; Urade, Miyuki; Yamanishi, Yukari; Chen, Xinyu
Journal of the Chemical Society, Perkin Transactions 2, 2002 , # 8 p. 1449 - 1454
参考文献
Montagne
Recueil des Travaux Chimiques des Pays-Bas, 1900 , vol. 19, p. 55
参考文献
Montagne
Recueil des Travaux Chimiques des Pays-Bas, 1900 , vol. 19, p. 55
反应条件
hydrogenchloride; tin(ll) chloride in ethanol T=20°C; Reduction;
参考文献
HETERO RESEARCH FOUNDATION; PARTHASARADHI REDDY, Bandi; RATHNAKAR REDDY, Kura; MURALIDHARA REDDY, Dasari; JANAKIRAM REDDY, Maruthi; VAMSI KRISHNA, Bandi
Patent: WO2012/46244 A1, 2012 ;
Location in patent: Page/Page column 6 ;
反应条件
potassium carbonate in dimethyl sulfoxide
参考文献
Rohm and Haas Company
Patent: US4259510 A1, 1981 ;
