4,4'-二溴-2,2'-并噻吩合成路线 (共 3 条)
反应条件
lithium diisopropyl amide in tetrahydrofuran
T=-70°C; Inert atmosphere;
参考文献
BASF SE; Kirner, Hans Jürg; Bienewald, Frank; Flores, Jean-Charles; Aebischer, Olivier Frédéric
Patent: US8436208 B2, 2013 ;
Location in patent: Page/Page column 32; 33 ;
反应条件
copper dichloride in diethyl ether
T=-78°C; 2 h;
参考文献
Dahlmann, Uwe; Neidlein, Richard
Helvetica Chimica Acta, 1996 , vol. 79, # 3 p. 755 - 766
反应条件
n-butyllithium; copper dichloride in diethyl ether
T=-70°C; Inert atmosphere;
参考文献
Parenti, Francesca; Morvillo, Pasquale; Bobeico, Eugenia; Diana, Rosita; Lanzi, Massimiliano; Fontanesi, Claudio; Tassinari, Francesco; Schenetti, Luisa; Mucci, Adele
European Journal of Organic Chemistry, 2011 , # 28 p. 5659 - 5667