N'-硝基-L-精氨酸甲酯盐酸盐合成路线 （共 5 条）
反应条件
trifluoroacetic acid in dichloromethane
参考文献
THE UNIVERSITY OF QUEENSLAND; FAIRLIE, David; REID, Robert C.
Patent: WO2013/67578 A1, 2013 ;
Location in patent: Page/Page column 102 ;
反应条件
thionyl chloride T=0 - 20°C;
参考文献
Zhou, Yinjian; Zhao, Ming; Wu, Yingting; Li, Chunyu; Wu, Jianhui; Zheng, Meiqing; Peng, Li; Peng, Shiqi
Bioorganic and Medicinal Chemistry, 2010 , vol. 18, # 6 p. 2165 - 2172
反应条件
1: sodium carbonate / N,N-dimethyl-formamide 2: trifluoroacetic acid / dichloromethane View Scheme
参考文献
THE UNIVERSITY OF QUEENSLAND; FAIRLIE, David; REID, Robert C.
Patent: WO2013/67578 A1, 2013 ;
反应条件
1: NO2/HNO3, SO3/H2SO4 2: SOCl2 View Scheme
参考文献
Gibian,H.; Schroeder,E.
Justus Liebigs Annalen der Chemie, 1961 , vol. 642, p. 145 - 162
反应条件
1: 1.) triethylamine / dioxane / 1.) RT, 1 h, 2.) RT, 12 h 2: hydrogen, HCl / PdCl2 / methanol / Ambient temperature View Scheme
参考文献
Synthetic Communications, , vol. 13, # 2 p. 167 - 176
