1-氯-2-甲基-1-丙烯合成路线 （共 91 条）
参考文献
Tischtschenko
Zhurnal Obshchei Khimii, 1938 , vol. 8, p. 1239
Chem.Abstr., 1939 , p. 4190
Chem. Zentralbl., 1939 , vol. 110, # II p. 4222
反应条件
(dcypb)PdMe2 in N,N-dimethyl-formamide
T=120°C; 2 h;
参考文献
Reetz, Manfred T.; Wanninger, Klaus; Hermes, Marcus
Chemical Communications, 1997 , # 6 p. 535 - 536
反应条件
Ni(dmpe)Cl2 in diethyl ether
参考文献
The University of Akron
Patent: US5245098 A1, 1993 ;
反应条件
1: 1-bromo-2-(1,3-dioxolan-2-yl)-benzene With iodine; magnesium in tetrahydrofuran
2 h; Inert atmosphereReflux;
2: 1-chloro-2-methyl-propene With copper(l) iodide in tetrahydrofuran
T=0 - 20°C;
3: With toluene-4-sulfonic acid in tetrahydrofuran; dichloromethane; water; acetone
2 h; Reflux;
参考文献
Beletskiy, Evgeny V.; Sudheer; Douglas, Christopher J.
Journal of Organic Chemistry, 2012 , vol. 77, # 14 p. 5884 - 5893
反应条件
pyridine; bromine in dichloromethane
参考文献
Beit-Yannai, Michal; Rappoport, Zvi; Shainyan, Bagrat A.; Danilevich, Yuri S.
Journal of Organic Chemistry, 1997 , vol. 62, # 23 p. 8049 - 8057
反应条件
n-butyllithium; N,N,N',N,-tetramethylethylenediamine in tetrahydrofuran; diethyl ether
T=-78°C; 6 h;
参考文献
Nelson, Donna J.; Nagarajan, Ananthanarayanan
Journal of Organometallic Chemistry, 1993 , vol. 463, # 1-2 p. 1 - 6
参考文献
Scheschukow
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1884 , vol. 16, p. 495
反应条件
N,N,N',N,-tetramethylethylenediamine in tetrahydrofuran; diethyl ether
T=-78°C; 6 h;
参考文献
Nelson, Donna J.; Nagarajan, Ananthanarayanan
Journal of Organometallic Chemistry, 1993 , vol. 463, # 1-2 p. 1 - 6
反应条件
(dcypb)PdMe2 in N,N-dimethyl-formamide
T=120°C; 2 h;
参考文献
Reetz, Manfred T.; Wanninger, Klaus; Hermes, Marcus
Chemical Communications, 1997 , # 6 p. 535 - 536
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; benzene
15 h; Heating;
参考文献
Ratovelomanana, Victorin; Linstrumelle, Gerard
Synthetic Communications, 1984 , vol. 14, # 2 p. 179 - 188
