2,3-二甲基-1,3-丁二烯合成路线 （共 777 条）
参考文献
Akkari, Rhalid; Calmes, Monique; Escale, Francoise; Iapichella, Julien; Rolland, Marc; Martinez, Jean
Tetrahedron Asymmetry, 2004 , vol. 15, # 16 p. 2515 - 2525
反应条件
triphenylmethane tetrafluoroborate in dichloromethane T=20°C; Diels-Alder Cycloaddition; 48 h;
参考文献
Bah, Juho; Franzen, Johan
Chemistry - A European Journal, 2014 , vol. 20, # 4 p. 1066 - 1072
反应条件
aluminum trisphenoxide polymer in toluene T=0°C; 18 h;
参考文献
Saito, Susumu; Murase, Masaaki; Yamamoto, Hisashi
Synlett, 1999 , # 1 p. 57 - 58
反应条件
hydrogen bromide 1.) benzene, 25 deg C, 1.5 h, 2.) CH2Cl2, from -78 deg C to -35 deg C, 20 min; Yield given. Multistep reaction;
参考文献
Wulff, William D.; Yang, Dominic C.
Journal of the American Chemical Society, 1983 , vol. 105, # 22 p. 6726 - 6727
反应条件
1: 60 percent / m-chloroperbenzoic acid, sodium carbonate / CH2Cl2 / 0 °C 2: 1.) Fe(CO)5, 2.) cerium(IV) ammonium nitrate / 1.) benzene, irradiated, room temperature, 2.) aq. ethanol, room temperature View Scheme
参考文献
Annis, Gary D.; Ley, Steven V.; Self, Christopher R.; Sivaramakrishnan, Ramamoorthy
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 270 - 277
反应条件
T=120°C; 7 h; Product distribution;
参考文献
Sennyey, Gerard; Mathey, Francois
Tetrahedron Letters, 1981 , vol. 22, # 47 p. 4713 - 4716
反应条件
in cyclohexane Kinetics; Irradiation (UV/VIS); 110-W low pressure Hg arc, under Ar, room temp.; GC-MS;
参考文献
Mochida, Kunio; Yoneda, Isao; Wakasa, Masanobu
Journal of Organometallic Chemistry, 1990 , vol. 399, # 1/2 p. 53 - 62
反应条件
in cyclohexane Irradiation (UV/VIS); irradiation of catenate in cyclohexane containing an excess of 2,3-dimethylbutadiene with a 110 W low-pressure Hg arc lamp at room temp. under Ar for 1-4 h, further products; identification by GC and GC-MS;
参考文献
Mochida, Kunio; Kikkawa, Haruhiko; Nakadaira, Yasuhiro
Journal of Organometallic Chemistry, 1991 , vol. 412, # 1.2 p. 9 - 19
反应条件
in cyclohexane Irradiation (UV/VIS); irradiation of catenate in cyclohexane containing an excess of 2,3-dimethylbutadiene with a 110 W low pressure Hg arc lamp at room temp. under Ar for 1-4 h, further products; identification by GC and GC-MS;
参考文献
Mochida, Kunio; Kikkawa, Haruhiko; Nakadaira, Yasuhiro
Journal of Organometallic Chemistry, 1991 , vol. 412, # 1.2 p. 9 - 19
反应条件
[(C6H10)(NCH(C6H2)(O)(tBu)2)2Cr]BF4 in toluene T=25°C; P=750.075 Torr; 24 h; Product distribution; Further Variations:SolventsPressuresCatalysts;
参考文献
Kwiatkowski, Piotr; Asztemborska, Monika; Caille, Jean-Claude; Jurczak, Janusz
Advanced Synthesis and Catalysis, 2003 , vol. 345, # 4 p. 506 - 509
