2,3-二甲基-1,3-丁二烯合成路线 （共 777 条）
反应条件
in benzene stirred for 6 h at 70°C; volatiles removed (vac.), chromy. (silica gel, hexane);
参考文献
Fukaya, Norihisa; Ichinohe, Masaaki; Sekiguchi, Akira
Angewandte Chemie - International Edition, 2000 , vol. 39, # 21 p. 3881 - 3884
反应条件
bis(η3-allyl)palladium-triisopropylphosphine in toluene T=110°C; 42 h; Further byproducts given;
参考文献
Deohring, A.; Jolly, P. W.
Tetrahedron Letters, 1980 , vol. 21, p. 3021 - 3024
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; thiourea; potassium iodide; nickel dichloride; zinc T=50°C; 1.5 h;
参考文献
Takagi; Mimura; Inokawa
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 12 p. 3517 - 3522
反应条件
potassium tert-butylate in N,N-dimethyl acetamide T=50°C; 3 h;
参考文献
Garst, Michael E.; Dolby, Lloyd J.; Esfandiari, Shervin; Okrent, Rachel A.; Avey, Alfred A.
Journal of Organic Chemistry, 2006 , vol. 71, # 2 p. 553 - 556
反应条件
n-butyllithium; potassium tert-butylate in hexane
参考文献
Ogle, Craig A.; Black, Kristyna C.; Sims, Philip F.
Journal of Organic Chemistry, 1992 , vol. 57, # 12 p. 3499 - 3503
反应条件
bis(η3-allyl)palladium-bisdicyclohexylphosphino-ethene in toluene T=90°C; 72 h; Further byproducts given;
参考文献
Deohring, A.; Jolly, P. W.
Tetrahedron Letters, 1980 , vol. 21, p. 3021 - 3024
参考文献
Courtot
Bulletin de la Societe Chimique de France, 1906 , vol. <3>35, p. 970,971,972
Full Text Show Details
Chupotsky; Marioza
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1889 , vol. 21, p. 432
反应条件
bis(η3-allyl)palladium-bisdicyclohexylphosphino-ethene in toluene T=90°C; 72 h; Further byproducts given;
参考文献
Deohring, A.; Jolly, P. W.
Tetrahedron Letters, 1980 , vol. 21, p. 3021 - 3024
参考文献
Tzeng, Dongjaw; Weber, William P.
Journal of the American Chemical Society, 1980 , vol. 102, # 4 p. 1451
反应条件
in 2-methyl cyclohexane Irradiation;
参考文献
Masamune,S.; Murakami,S.; Tobita,H.
Journal of the American Chemical Society, 1983 , vol. 105, p. 7776
