2,3-二甲基-1,3-丁二烯合成路线 (共 777 条)
反应条件
in hexane T=-70°C; 20 h; UV-irradiation;
参考文献
Hurni, Krysten L.; Baines, Kim M.
Canadian Journal of Chemistry, 2007 , vol. 85, # 10 p. 668 - 674
反应条件
1: With carbon monoxide; {Pd([1,10]phenanthroline)2}[BF4]2; triethylamine in tetrahydrofuran T=100°C; P=7500.75 Torr; 6 h; 2: in benzene T=200°C; P=7500.75 Torr; 3 h; Further stages. Title compound not separated from byproducts.;
参考文献
Ragaini, Fabio; Cenini, Sergio; Brignoli, Daniela; Gasperini, Michela; Gallo, Emma
Journal of Organic Chemistry, 2003 , vol. 68, # 2 p. 460 - 466
反应条件
T=500°C; P=0.001 Torr;
参考文献
Kwak, Young-Woo; Jeong, Ill-Hyeon; Ko, Jae-You; Boo, Bong Hyun
Journal of Organometallic Chemistry, 1992 , vol. 439, # 2 p. 107 - 113
参考文献
Burns, Gary T.; Barton, Thomas J.
Journal of the American Chemical Society, 1983 , vol. 105, # 7 p. 2006 - 2009
反应条件
T=700°C; P=0.001 Torr; other alkoxy- and deuterated analogues, other temp.; Product distributionMechanism;
参考文献
Journal of Organometallic Chemistry, , vol. 439, # 2 p. 107 - 113
反应条件
in pentane Irradiation (UV/VIS); (N2), 1 h irradiated; gas chromatography; elem. anal., NMR, mass. spectra;
参考文献
Organometallics, , vol. 10, p. 2772 - 2777
反应条件
in pentane Irradiation (UV/VIS); (N2), 1 h irradiated; gas chromatography; elem. anal., NMR, mass. spectra;
参考文献
Organometallics, , vol. 10, p. 2772 - 2777
反应条件
in pentane Irradiation (UV/VIS); (N2), 1.5 h irradiated; column chromatography; elem. anal., NMR, mass. spectra;
参考文献
Organometallics, , vol. 10, p. 2772 - 2777
反应条件
in cyclohexane Irradiation (UV/VIS); irradiation of catenate in cyclohexane containing an excess of 2,3-dimethylbutadiene with a 110 W low pressure Hg arc lamp at room temp. under Ar for 1-4 h; identification by GC and GC-MS;
参考文献
Journal of Organometallic Chemistry, , vol. 412, # 1.2 p. 9 - 19
反应条件
in not given thermal reaction; main product Os3(CO)12;;
参考文献
Polyhedron, , vol. 7, p. 931 - 942