2,3-二甲基-1,3-丁二烯合成路线 （共 777 条）
反应条件
in neat (no solvent) Irradiation (UV/VIS); Ge deriv. and a large excess of organic reagent irradiating in a quartztube for 4 h then concg. in vacuo; identified by high-pressure chromy. and NMR spectra;
参考文献
Riviere, P.; Castel, A.; Satge, J.; Guyot, D.
Journal of Organometallic Chemistry, 1984 , vol. 264, # 1-2 p. 193 - 206
反应条件
bismuth(III) chloride in chloroform T=60°C; 3.5 h; Yield given. Yields of byproduct given;
参考文献
Robert, Helene; Garrigues, Bernard; Dubac, Jacques
Tetrahedron Letters, 1998 , vol. 39, # 10 p. 1161 - 1164
反应条件
bis(1,5-cyclooctadiene)nickel (0); tri-cyclo-hexyl-phosphine in toluene T=130°C; 48 h; Inert atmosphere;
参考文献
Ohashi, Masato; Takeda, Ippei; Ikawa, Masashi; Ogoshi, Sensuke
Journal of the American Chemical Society, 2011 , vol. 133, # 45 p. 18018 - 18021
反应条件
bis(1,5-cyclooctadiene)nickel (0); tri-cyclo-hexyl-phosphine in deuterated toluene T=130°C; 62 h; Inert atmosphere;
参考文献
Ohashi, Masato; Takeda, Ippei; Ikawa, Masashi; Ogoshi, Sensuke
Journal of the American Chemical Society, 2011 , vol. 133, # 45 p. 18018 - 18021
反应条件
bis(1,5-cyclooctadiene)nickel (0); tri-cyclo-hexyl-phosphine in deuterated toluene T=130°C; 23 h; Inert atmosphere;
参考文献
Ohashi, Masato; Takeda, Ippei; Ikawa, Masashi; Ogoshi, Sensuke
Journal of the American Chemical Society, 2011 , vol. 133, # 45 p. 18018 - 18021
反应条件
BPTC in dimethyl sulfoxide T=150°C; 6 h;
参考文献
Sato, Ryu; Satoh, Shin-ichi; Saito, Minoru
Chemistry Letters, 1990 , p. 139 - 142
反应条件
bromine; acetic acid
参考文献
Kondakow
Journal fuer Praktische Chemie (Leipzig), 1900 , vol. <2>62, p. 171
反应条件
bromine in dichloromethane T=-78°C; 5 h;
参考文献
Farkas, Frederic; Wellauer, Thomas; Esser, Thomas; Sequin, Urs
Helvetica Chimica Acta, 1991 , vol. 74, # 7 p. 1511 - 1519
反应条件
bromine T=60°C; 0.5 h;
参考文献
Collier,W.L.; Macomber,R.S.
Journal of Organic Chemistry, 1973 , vol. 38, p. 1367 - 1369
参考文献
Sweeting; Johnson
Journal of the American Chemical Society, 1946 , vol. 68, p. 1060
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Farmer; Lawrence; Scott
Journal of the Chemical Society, 1930 , p. 521
Full Text Show Details
Kogerman
Sber.Naturf.-Ges.Tartu, 1934 , vol. 41, p. 281
Chem. Zentralbl., 1935 , vol. 106, # I p. 2965
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Jessafow
Zhurnal Obshchei Khimii, 1949 , vol. 19, p. 1070
Chem.Abstr., 1950 , p. 1001
