2,3-二甲基-1,3-丁二烯合成路线 (共 777 条)
反应条件
Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bestmann, Hans Juergen; Roeder, Thomas; Suehs, Kurt
Chemische Berichte, 1988 , vol. 121, p. 1509 - 1518
反应条件
(i) Hg(OAc)2, H2O, THF, (ii) aq. NaOH, NaBH4; Multistep reaction;
参考文献
Brown,H.C. et al.
Journal of Organic Chemistry, 1972 , vol. 37, # 12 p. 1941 - 1947
反应条件
1: benzene-d6 2: benzene View Scheme
参考文献
Tsumuraya, Takeshi; Sadao, Sato; Ando, Wataru
Organometallics, 1989 , vol. 8, p. 161 - 167
反应条件
1: benzene-d6 2: benzene View Scheme
参考文献
Tsumuraya, Takeshi; Sadao, Sato; Ando, Wataru
Organometallics, 1989 , vol. 8, p. 161 - 167
反应条件
in toluene Heatingother solvent, temperature, reaction time; Product distribution;
参考文献
Tardif, Sylvie L.; Rys, Andrzej Z.; Abrams, Charles B.; Abu-Yousef, Imad A.; Leste-Lasserre, Pierre B. F.; Schultz, Erwin K. V.; Harpp, David N.
Tetrahedron, 1997 , vol. 53, # 36 p. 12225 - 12236
反应条件
Tl(NO3)3*3H2O in methanol; dichloromethane 1 h; Ambient temperature;
参考文献
Chemistry Letters, , p. 997 - 1000
反应条件
Tl(NO3)3*3H2O in methanol; dichloromethane 1 h; Ambient temperature;
参考文献
Chemistry Letters, , p. 997 - 1000
反应条件
tert.-butyl lithium in pentane T=-20°C;
参考文献
Auner, N.
Journal of Organometallic Chemistry, 1987 , vol. 336, p. 83 - 104
反应条件
hydrogen; zirconium tetra-n-butoxide; diethylaluminium chloride; nickel; triphenylphosphine 1.) toluene, 100 deg C, 8 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Dzhemilev, U. B.; Ibragimov, A. G.; Tolstikov, G. A.; Vostrikova, O. S.; Zelenova, L. M.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # 11 p. 2066 - 2071
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 11 p. 2313 - 2319
参考文献
Holmes et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 141